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4-(Trimethylsilyl)morpholine

Product Name 4-(Trimethylsilyl)morpholine

CAS13368-42-8

MFC7H17NOSi

MW159.3

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  • Mass 

    MS-NW-9945          
4-(trimethylsilyl)morpholine
C7H17NOSi           (Mass of molecular ion:    159)


       Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV


          15.0       1.5
      27.0       3.4
      28.0      15.7
      29.0      19.4
      30.0       8.4
      31.0       4.1
      41.0       2.6
      42.0       7.4
      43.0      11.3
      44.0       4.8
      45.0      22.3
      46.0       1.5
      47.0       2.2
      52.0       1.2
      54.0       1.8
      55.0       6.6
      56.0      13.4
      57.0      28.9
      57.5       2.1
      58.0       6.3
      59.0      52.4
      60.0       4.1
      61.0       3.3
      66.0       2.9
      70.0       3.7
      71.0       2.1
      72.0       4.1
      73.0      81.0
      74.0       7.3
      75.0      22.8
      76.0       1.7
      77.0       2.4
      85.0       1.7
      86.0     100.0
      87.0      32.3
      88.0       5.3
      89.0       2.4
      93.0       1.2
     100.0      16.8
     101.0      83.4
     102.0      10.2
     103.0       9.8
     114.0      13.5
     115.0       2.3
     116.0       1.6
     128.0       1.6
     129.0      11.0
     130.0       2.0
     131.0       2.2
     144.0      74.5
     145.0       9.2
     146.0       3.5
     147.0      34.7
     148.0       5.5
     149.0       3.3
     158.0      20.2
     159.0      71.6
     160.0      11.2
     161.0       3.3
     229.0       1.5

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H17 N O Si 0.05 ml : 0.5 ml CDCl3
    4-(trimethylsilyl)morpholine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             3.550
      B             2.827
      C             0.044
  

         Hz     ppm     Int.


       1423.71   3.563    139
   1419.19   3.552    154
   1414.43   3.540    163
   1134.64   2.840    150
   1129.88   2.828    158
   1125.24   2.816    159
     22.22   0.056     47
     21.24   0.054     76
     17.82   0.045   1000
     14.77   0.037    144

in CDCl3



liquid film





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