ALPHA,ALPHA'-DIANILINO-P-XYLENE
Product Name ALPHA,ALPHA'-DIANILINO-P-XYLENE
CAS13170-62-2
MFC20H20N2
MW288.39
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MassMS-IW-4053 N,N'-(p-phenylenedimethylene)dianiline C20H20N2 (Mass of molecular ion: 288)
Source Temperature: 180 °C Sample Temperature: 160 °C Direct, 75 eV
28.0 1.0 39.0 2.3 51.0 4.1 52.0 1.0 63.0 1.2 65.0 7.6 66.0 3.4 77.0 25.3 78.0 6.3 79.0 5.6 89.0 3.3 90.0 3.2 91.0 20.6 92.0 7.4 93.0 12.8 94.0 2.2 103.0 5.4 104.0 48.8 105.0 12.6 106.0 7.4 117.0 1.6 118.0 4.0 119.0 1.9 130.0 1.0 143.0 1.9 143.5 3.2 144.0 9.7 144.5 2.1 152.0 1.0 156.0 1.2 165.0 1.1 167.0 2.3 168.0 1.2 178.0 1.3 179.0 2.5 180.0 5.6 181.0 7.9 182.0 6.3 183.0 2.3 193.0 2.1 194.0 21.5 195.0 27.6 196.0 100.0 197.0 19.1 198.0 1.7 283.0 1.5 284.0 2.7 285.0 1.3 286.0 6.2 287.0 7.2 288.0 83.4 289.0 18.7 290.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C20 H20 N2 0.030 g : 0.5 ml CDCl3 N,N'-(p-phenylenedimethylene)dianiline 
Assign. Shift(ppm)
A 7.323 B 7.159 C 6.706 D 6.610 E 4.290 F 3.98
Hz ppm Int.2926.64 7.324 1000 2869.63 7.181 187 2868.77 7.179 81 2867.55 7.176 65 2864.50 7.168 41 2862.30 7.163 252 2860.96 7.159 252 2858.89 7.154 41 2855.59 7.146 74 2854.49 7.143 94 2853.64 7.141 223 2851.44 7.135 34 2688.23 6.727 47 2687.13 6.724 83 2686.16 6.722 52 2680.79 6.708 82 2679.81 6.706 150 2678.83 6.703 87 2673.58 6.690 43 2672.49 6.688 73 2671.51 6.685 45 2646.97 6.624 203 2645.87 6.621 238 2643.92 6.616 72 2639.28 6.604 130 2638.31 6.602 225 2637.33 6.600 189 2635.01 6.594 32 1714.60 4.291 301 1593.02 3.987 37
in CDCl3
KBr disc
nujol mull
