4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE
Product Name 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE
CAS13104-56-8
MFC22H17N3O
MW339.39
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MassMS-NW-6975 4-(p-methoxyphenyl)-2,6-di(2-pyridyl)pyridine C22H17N3O (Mass of molecular ion: 339)
Source Temperature: 200 °C Sample Temperature: 150 °C Direct, 75 eV
18.0 1.5 51.0 2.8 52.0 1.0 63.0 1.2 78.0 5.2 79.0 1.2 89.0 1.1 95.5 1.1 134.0 1.4 134.5 1.0 135.0 1.3 140.0 1.0 147.0 1.6 147.5 2.7 148.0 5.1 148.5 1.4 153.5 1.5 162.0 1.6 164.0 1.0 169.5 6.0 170.0 1.7 190.0 1.7 191.0 3.2 192.0 1.6 216.0 1.4 217.0 2.0 218.0 4.1 219.0 1.1 234.0 2.2 246.0 1.2 261.0 7.3 262.0 1.5 267.0 1.0 268.0 2.6 269.0 1.4 294.0 2.3 295.0 5.6 296.0 7.2 297.0 2.2 308.0 3.7 309.0 2.1 310.0 1.1 311.0 2.7 323.0 1.2 324.0 14.3 325.0 3.7 338.0 7.6 339.0 100.0 340.0 24.9 341.0 3.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C22 H17 N3 O 0.033 g : 0.5 ml CDCl3 4-(p-methoxyphenyl)-2,6-di(2-pyridyl)pyridine 
Assign. Shift(ppm)
A 8.66 B 8.66 C 8.60 D 7.82 E 7.81 F 7.27 G 6.973 J 3.809
Hz ppm Int.779.50 8.704 135 778.56 8.694 142 777.63 8.683 158 775.31 8.657 845 767.75 8.573 148 766.75 8.562 193 765.75 8.551 125 760.88 8.496 31 707.25 7.897 104 705.13 7.874 239 702.88 7.849 84 699.69 7.813 170 697.81 7.792 190 696.13 7.773 259 693.06 7.739 62 691.94 7.726 107 690.00 7.705 102 657.88 7.346 107 656.50 7.331 99 653.19 7.294 97 651.81 7.278 112 650.38 7.262 94 649.13 7.248 85 644.38 7.195 78 631.44 7.051 37 628.44 7.017 230 626.25 6.993 69 621.63 6.941 69 619.50 6.918 179 341.19 3.810 1000
in CDCl3
KBr disc
nujol mull
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