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2-Methylbenzophenone

Product Name 2-Methylbenzophenone

CAS131-58-8

MFC14H12O

MW196.24

¹³CNMR

Mass

MS-NW-6014          
2-methylbenzophenone
C14H12O             (Mass of molecular ion:    196)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       1.3
      28.0       1.1
      39.0       7.0
      41.0       1.9
      50.0       3.5
      51.0      12.1
      52.0       1.2
      62.0       1.6
      63.0       5.0
      64.0       1.5
      65.0      14.7
      74.0       1.4
      75.0       1.5
      76.0       3.0
      77.0      31.7
      78.0       2.5
      82.0       1.6
      82.5       1.4
      83.0       1.6
      88.5       1.4
      89.0       7.0
      90.0       3.1
      90.5       1.1
      91.0      34.8
      92.0       3.0
      97.0       2.3
      97.5       1.2
     105.0      25.2
     106.0       2.2
     115.0       1.1
     118.0       1.1
     119.0      31.0
     120.0       2.7
     152.0       3.3
     153.0       1.3
     165.0       5.9
     166.0       1.7
     167.0       2.9
     177.0       5.2
     178.0       7.9
     179.0       7.0
     180.0       1.1
     181.0       6.1
     182.0       1.2
     194.0       4.4
     195.0     100.0
     196.0      68.3
     197.0       9.5

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₂ O	0.05 ml : 0.5 ml CDCl₃
2-methylbenzophenone

    Assign.     Shift(ppm)

      A             7.792
      B             7.537
      C             7.418
      D             7.357
      E             7.287
      F             7.263
      G             7.216
      J             2.318

     Hz     ppm     Int.

   3120.36   7.808     49
   3118.65   7.804    245
   3118.04   7.802    213
   3117.31   7.801    337
   3112.30   7.788    104
   3110.23   7.783    376
   3108.89   7.780    371
   3022.22   7.563     49
   3020.87   7.559     97
   3019.53   7.556     60
   3015.38   7.546     65
   3013.43   7.541    205
   3011.60   7.536     86
   3007.45   7.526     93
   3006.10   7.522    167
   3004.76   7.519     95
   2973.27   7.440     61
   2971.56   7.436    256
   2970.09   7.432    133
   2967.90   7.427     31
   2967.41   7.426     31
   2963.62   7.416    350
   2962.40   7.413    147
   2958.01   7.402     84
   2956.30   7.398    186
   2955.69   7.396    145
   2954.83   7.394     71
   2949.83   7.382     68
   2948.24   7.378     77
   2942.26   7.363    137
   2940.67   7.359    169
   2934.94   7.344    116
   2933.35   7.340    137
   2918.09   7.302    109
   2916.63   7.298    125
   2910.40   7.283    193
   2908.94   7.279    187
   2906.86   7.274    174
   2906.13   7.272    206
   2905.52   7.271    198
   2899.17   7.255    120
   2898.56   7.253    140
   2897.95   7.252    130
   2890.87   7.234    133
   2890.14   7.232    126
   2883.06   7.214    150
   2882.57   7.213    146
   2876.59   7.198     54
   2875.98   7.197     65
   2875.37   7.195     65
   2874.88   7.194     57
    926.51   2.319   1000
    920.65   2.304     49

¹H NMR	89.56 MHz
C₁₄ H₁₂ O	0.05 ml : 0.5 ml CDCl₃
2-methylbenzophenone

    Assign.     Shift(ppm)

      A             7.79
      B          7.58 to 7.16
      C             2.318

     Hz     ppm     Int.

    702.88   7.849    133
    701.25   7.830    159
    699.88   7.815     82
    699.00   7.805     81
    697.44   7.788     85
    695.31   7.764    193
    693.19   7.740    226
    684.25   7.641     32
    682.38   7.620     30
    677.25   7.562     74
    676.44   7.553     91
    673.56   7.521     84
    672.50   7.509    157
    670.31   7.485    304
    668.31   7.463    159
    665.69   7.433    104
    664.00   7.415    122
    662.38   7.396    190
    659.75   7.367    119
    655.25   7.317    206
    654.00   7.303    312
    652.00   7.281    471
    650.50   7.264    307
    647.75   7.233    156
    643.06   7.181     58
    207.88   2.322   1000

in CDCl3

liquid film

4880 A,200 M,liquid

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