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129041-31-2More Spectrum > N,N-BIS(3-CHLOROBENZYL)AMINE(129041-31-2)1HNMR
N,N-BIS(3-CHLOROBENZYL)AMINE
Product Name N,N-BIS(3-CHLOROBENZYL)AMINE
CAS129041-31-2
MFC14H13Cl2N
MW266.17
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MassMS-IW-8355 bis(3-chlorobenzyl)amine C14H13Cl2N (Mass of molecular ion: 265)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 2.1 50.0 1.8 51.0 2.6 63.0 4.2 65.0 1.9 73.0 1.3 75.0 3.2 76.0 1.1 77.0 5.4 89.0 14.0 90.0 6.0 91.0 41.9 92.0 3.4 99.0 5.1 101.0 1.8 102.0 1.5 106.0 1.7 111.0 1.8 112.0 1.3 113.0 3.0 115.0 1.0 117.0 1.3 125.0 100.0 126.0 30.4 127.0 34.2 128.0 9.9 137.0 3.9 138.0 3.1 139.0 2.7 140.0 99.9 141.0 8.8 142.0 31.9 143.0 2.7 152.0 6.0 153.0 1.0 154.0 17.2 155.0 1.7 156.0 4.9 230.0 3.3 232.0 1.0 262.0 1.7 263.0 2.4 264.0 9.3 265.0 8.2 266.0 6.6 267.0 4.6 268.0 1.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H13 Cl2 N 0.05 ml : 0.5 ml CDCl3 bis(3-chlorobenzyl)amine 
Assign. Shift(ppm)
A 7.325 B 7.22 to 7.19 C 3.730 D 1.61
Hz ppm Int.2929.57 7.331 299 2927.73 7.326 468 2897.09 7.250 69 2889.77 7.231 264 2889.28 7.230 241 2885.13 7.220 348 2883.42 7.215 711 2882.57 7.213 1000 2880.62 7.208 483 2877.08 7.200 165 2875.37 7.195 355 2873.90 7.192 306 2873.29 7.190 272 2871.83 7.186 183 2869.14 7.180 111 2868.29 7.178 95 2867.19 7.175 135 2866.70 7.174 138 2865.11 7.170 95 1490.97 3.731 988 642.70 1.609 133
in CDCl3
liquid film
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