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Titanocene dichloride

Product Name Titanocene dichloride

CAS1271-19-8

MFC10H10Cl2Ti

MW248.96

Mass

MS-NW-2436          
titanocene dichloride
C10H10Cl2Ti         (Mass of molecular ion:    248)

   Source Temperature: 200 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       3.1
      28.0       1.7
      36.0       2.1
      37.0       1.0
      38.0       3.3
      39.0      30.6
      40.0       2.2
      48.0       1.7
      62.0       1.6
      63.0       4.0
      64.0       1.3
      65.0      26.7
      66.0       4.9
      73.0       1.5
      81.0       1.3
      82.0       1.3
      83.0      13.1
      84.0       1.6
      85.0       6.0
      86.0       2.2
      87.0       1.1
     108.0       1.4
     110.0       1.1
     112.0       1.6
     113.0       1.7
     116.0       1.0
     117.0       1.0
     118.0      10.1
     119.0       1.5
     120.0       7.4
     121.0       3.5
     122.0       6.4
     123.0       1.9
     124.0       2.4
     128.0       1.3
     146.0       4.7
     147.0       6.6
     148.0      38.8
     149.0       7.2
     150.0      15.0
     151.0       1.9
     152.0       1.1
     176.0       2.3
     178.0       1.5
     181.0      10.1
     182.0      10.1
     183.0     100.0
     184.0      18.3
     185.0      67.2
     186.0       9.2
     187.0      13.8
     188.0       1.4
     211.0       2.1
     212.0       3.7
     213.0      11.1
     214.0       3.1
     215.0       4.0
     246.0       2.1
     247.0       2.1
     248.0      20.1
     249.0       4.7
     250.0      13.5
     251.0       2.5
     252.0       2.9

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₀ H₁₀ Cl₂ Ti	0.038 g : 0.5 ml DMSO-d₆
titanocene dichloride

    Assign.     Shift(ppm)

      A             6.673

     Hz     ppm     Int.

   2671.26   6.684     33
   2667.11   6.674   1000

KBr disc

TI(III) COMPLEX IN C6H6/(CH3)C6H5, X-BAND

GRIGNARD REACTION WITH PROPYLENE IN THF

REDUCTION WITH NA AND ALCL3 IN THF

TI(III) COMPLEX IN C6H6/(CH3)C6H5, Q-BAND

TI(III) COMPLEX IN C6H6/(CH3)C6H5, HALF FIELD

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