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MS-IW-1369 1-chloro-2-propanol C3H7ClO (Mass of molecular ion: 94)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 4.9 18.0 1.6 19.0 6.3 26.0 1.5 27.0 12.8 28.0 3.7 29.0 7.1 31.0 43.9 36.0 1.7 38.0 1.0 39.0 3.5 41.0 6.6 42.0 1.9 43.0 20.5 44.0 1.7 45.0 100.0 46.0 3.2 49.0 3.0 51.0 1.0 57.0 3.1 58.0 2.6 59.0 1.2 62.0 4.2 63.0 3.8 64.0 1.4 65.0 3.6 77.0 1.6 79.0 14.9 81.0 4.8 93.0 1.1 95.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C3 H7 Cl O 0.05 ml : 0.5 ml CDCl3 1-chloro-2-propanol Assign. Shift(ppm)
A 4.01 B *1 3.567 C *1 3.472 D 3.22 E 1.272 J(A,B)=4.0HZ J(A,C)=6.7HA J(B,C)=-11.0HZ
Hz ppm Int.
1608.28 4.025 41 1605.10 4.017 52 1602.17 4.009 60 1598.75 4.001 54 1595.95 3.994 44 1592.41 3.985 31 1434.33 3.589 181 1430.30 3.579 177 1423.34 3.562 294 1419.31 3.552 275 1395.39 3.492 384 1388.67 3.475 337 1384.40 3.465 246 1377.69 3.448 237 1284.67 3.215 100 511.47 1.280 1000 508.06 1.272 46 505.13 1.264 959
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