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123071-42-1

MALONALDEHYDE DIANILIDE HYDROCHLORIDE

Product Name MALONALDEHYDE DIANILIDE HYDROCHLORIDE

CAS123071-42-1

MFC15H15ClN2

MW258.75

  • 123071-42-1_ms_1
    Mass

    MS-KW-0192          
    N-(3-anilinoallylidene)aniline monohydrochloride
    C15H14N2 HCl        (Mass of molecular ion:    222)
    

       Source Temperature: 180 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          18.0       1.1
          28.0       2.3
          35.0       1.4
          36.0      19.6
          38.0       6.9
          39.0       3.2
          50.0       1.8
          51.0      11.8
          52.0       2.1
          63.0       1.2
          65.0       3.9
          66.0       2.7
          76.0       2.0
          77.0      31.0
          78.0       4.0
          89.0       1.2
          90.0       1.9
          91.0       5.9
          92.0       2.4
          93.0       9.1
         102.0       2.7
         103.0       6.7
         104.0       7.8
         111.0       7.2
         111.5       1.2
         116.0       2.2
         117.0       5.4
         118.0       9.0
         119.0       3.2
         128.0       4.9
         129.0       8.7
         130.0      22.1
         131.0       2.4
         143.0       2.5
         144.0       3.1
         145.0      10.2
         146.0       1.1
         180.0       1.8
         193.0       1.1
         194.0       2.7
         195.0       1.9
         204.0       1.1
         205.0       1.0
         206.0       5.0
         219.0       4.2
         220.0       1.9
         221.0      99.2
         222.0     100.0
         223.0      15.9
         224.0       1.3
    

400 MHz in DMSO-d6

  • 123071-42-1_1hnmr_1

    1H NMR 399.65 MHz
    C15 H14 N2 0.038 g : 0.5 ml DMSO-d6
    N-(3-anilinoallylidene)aniline monohydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.8 B 9.056 C 7.48 D 7.25 E 6.589

         Hz     ppm     Int.
    

       5120.42  12.813     72
       3621.02   9.061     78
       3609.85   9.033     75
       2996.24   7.498    124
       2989.83   7.482   1000
       2987.81   7.477    516
       2983.42   7.466    365
       2978.29   7.453     50
       2976.64   7.449     62
       2974.62   7.444     87
       2906.12   7.272     66
       2904.10   7.267    106
       2901.17   7.260     86
       2899.89   7.257    105
       2897.69   7.251    122
       2895.50   7.246     95
       2891.65   7.236     66
       2889.27   7.230     44
       2645.11   6.619     53
       2633.57   6.590    102
       2622.03   6.561     50
    

in DMSO-d6

  • 123071-42-1_13cnmr_1

KBr disk

  • 123071-42-1_ir1_2

Nujol

  • 123071-42-1_ir2_1