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MS-IW-1311 thiomorpholine C4H9NS (Mass of molecular ion: 103)
Source Temperature: 250 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.7 26.0 1.4 27.0 5.9 28.0 21.1 29.0 25.6 30.0 20.9 40.0 1.1 41.0 4.5 42.0 33.2 43.0 3.9 44.0 9.0 45.0 8.0 46.0 17.3 47.0 4.1 48.0 1.6 54.0 1.8 55.0 2.0 56.0 46.9 57.0 85.3 58.0 4.3 59.0 4.4 60.0 1.3 61.0 8.8 74.0 6.3 75.0 5.0 88.0 27.7 89.0 1.3 90.0 1.3 102.0 2.9 103.0 100.0 104.0 6.4 105.0 4.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H9 N S 0.05 ml : 0.5 ml CDCl3 thiomorpholine Assign. Shift(ppm)
A 3.102 B 2.589 C 2.06
Hz ppm Int.
1244.87 3.115 924 1241.94 3.108 545 1239.75 3.103 816 1237.06 3.096 516 1234.50 3.089 927 1039.92 2.603 1000 1037.11 2.596 545 1034.67 2.589 876 1032.47 2.584 525 1029.42 2.576 876 825.07 2.065 496
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