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MS-NW-1323 3-methyl-1-butanol C5H12O (Mass of molecular ion: 88)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.9 18.0 2.0 19.0 3.0 26.0 1.7 27.0 25.7 28.0 10.0 29.0 32.8 31.0 35.5 38.0 1.5 39.0 18.1 40.0 3.1 41.0 59.9 42.0 87.1 43.0 69.0 44.0 3.0 45.0 17.5 46.0 8.3 47.0 1.6 53.0 2.4 54.0 1.3 55.0 100.0 56.0 11.8 57.0 25.4 58.0 1.2 69.0 5.6 70.0 69.7 71.0 5.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H12 O 0.02 ml : 0.5 ml CDCl3 3-methyl-1-butanol Assign. Shift(ppm)
A 3.673 B 1.66 C 1.57 D 1.49 E 0.922
Hz ppm Int.
335.75 3.749 164 329.00 3.674 299 327.31 3.655 35 322.31 3.599 170 154.69 1.728 37 148.63 1.660 42 143.19 1.599 36 140.63 1.571 253 137.38 1.534 43 136.94 1.530 41 134.38 1.501 184 127.63 1.426 128 121.50 1.357 37 120.19 1.343 31 85.25 0.952 1000 79.19 0.885 805
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