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MS-NW-2348 N(alpha)-acetyl-L-tryptophan C13H14N2O3 (Mass of molecular ion: 246)
Source Temperature: 280 °C Sample Temperature: 150 °C Direct, 75 eV
15.0 1.1 17.0 1.0 18.0 5.3 28.0 2.0 43.0 6.7 44.0 1.0 51.0 1.4 63.0 1.0 76.0 1.0 77.0 5.8 102.0 2.5 103.0 4.8 115.0 1.6 117.0 2.5 128.0 1.5 129.0 3.1 130.0 100.0 131.0 10.4 132.0 1.1 143.0 1.0 157.0 1.2 158.0 1.7 159.0 1.7 170.0 1.1 187.0 12.4 188.0 1.5 228.0 3.2 246.0 4.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C13 H14 N2 O3 0.041 g : 0.5 ml DMSO-d6 N(alpha)-acetyl-L-tryptophan Assign. Shift(ppm)
A 12.6 B 10.8 C 8.17 D 7.542 E 7.345 F 7.152 G 7.071 J 6.994 K 4.485 L *1 3.175 M *1 3.010 N 1.816
Hz ppm Int.
4330.97 10.837 93 3267.69 8.177 100 3260.00 8.158 103 3018.40 7.553 106 3010.52 7.533 116 2939.46 7.356 128 2932.31 7.338 109 2931.58 7.336 153 2859.78 7.156 158 2857.40 7.150 155 2834.68 7.093 55 2833.59 7.091 57 2827.72 7.076 96 2826.63 7.073 114 2819.67 7.056 78 2818.57 7.053 72 2802.45 7.013 86 2801.35 7.010 87 2795.30 6.995 86 2794.39 6.993 126 2793.66 6.991 96 2787.61 6.976 60 2786.51 6.973 56 1803.64 4.514 33 1798.51 4.501 43 1795.03 4.492 63 1790.45 4.481 62 1787.16 4.472 47 1782.03 4.459 36 1279.97 3.203 45 1275.02 3.191 48 1265.50 3.167 69 1260.37 3.154 65 1213.48 3.037 68 1204.87 3.015 69 1198.82 3.000 50 1190.22 2.979 46 725.89 1.817 1000
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