DIBENZOSUBERYL CHLORIDE

Mass

MS-IW-9261          
5-chloro-10,11-dihydro-5H-dibenzo(a,d)cycloheptene
C15H13Cl            (Mass of molecular ion:    228)

   Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      36.0       1.5
      63.0       1.1
      76.0       1.4
      81.5       1.0
      82.0       1.3
      82.5       4.1
      83.0       1.3
      89.0       5.1
      91.0       2.8
      94.0       1.0
      94.5       3.2
      95.0       2.0
      95.5       4.0
      96.0       3.0
      96.5       1.1
     115.0      14.2
     116.0       2.0
     152.0       1.7
     165.0       4.9
     176.0       1.1
     178.0      15.6
     179.0       4.3
     189.0       6.2
     190.0       3.1
     191.0      17.8
     192.0      13.3
     193.0     100.0
     194.0      19.6
     195.0       1.7

Assign. Shift(ppm) A 7.44 to 7.02 B 6.093 C *1 3.73 D *1 2.97

     Hz     ppm     Int.

    662.50   7.398     93
    660.19   7.372    137
    659.13   7.360    118
    658.25   7.350     96
    656.69   7.333    191
    655.69   7.322    196
    652.75   7.289    379
    649.75   7.255    292
    648.81   7.245    356
    646.38   7.218    878
    645.38   7.207   1000
    643.81   7.189    643
    642.38   7.173    420
    640.50   7.152    240
    638.31   7.128    139
    635.19   7.093     73
    545.19   6.088    408
    351.31   3.923     82
    345.94   3.863     58
    341.56   3.814     97
    339.69   3.793    112
    335.50   3.747    118
    333.25   3.721    121
    326.75   3.649    128
    325.88   3.639    142
    321.00   3.585     59
    275.38   3.075    144
    274.19   3.062    123
    267.75   2.990    131
    265.50   2.965    119
    261.56   2.921    106
    259.50   2.898    110
    255.13   2.849     61
    249.63   2.788     74