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MS-NW-8585 n-isopropylcyclohexylamine C9H19N (Mass of molecular ion: 141)
Source Temperature: 250 °C Sample Temperature: 130 °C Reservoir, 75 eV
18.0 2.3 27.0 5.8 28.0 6.2 29.0 3.6 30.0 5.3 39.0 4.7 41.0 14.2 42.0 5.5 43.0 9.8 44.0 51.1 45.0 1.4 53.0 1.9 54.0 2.4 55.0 12.0 56.0 36.5 57.0 2.5 58.0 6.0 67.0 1.4 68.0 1.3 70.0 16.8 71.0 1.3 72.0 1.9 79.0 1.1 81.0 2.4 82.0 1.8 83.0 3.2 84.0 3.8 85.0 6.0 98.0 100.0 99.0 7.4 112.0 3.3 126.0 32.2 127.0 3.0 140.0 1.6 141.0 14.8 142.0 2.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H19 N 0.05 ml : 0.5 ml CDCl3 N-isopropylcyclohexylamine Assign. Shift(ppm)
A 2.970 B 2.497 C 1.875 D 1.720 E 1.612 F 1.256 G 1.152 J 1.036 K 1.03 J(B,C)=3.8HZ J(B,K)=10.5HZ
Hz ppm Int.
1193.48 2.987 68 1187.26 2.971 91 1180.91 2.955 70 998.54 2.499 54 994.75 2.490 30 757.45 1.896 42 755.86 1.892 42 754.88 1.889 44 753.78 1.887 42 745.85 1.867 47 744.75 1.864 46 743.41 1.861 44 742.19 1.858 46 741.21 1.855 46 697.39 1.746 32 693.85 1.737 46 690.43 1.728 36 684.08 1.712 39 680.54 1.703 52 677.98 1.697 37 513.55 1.285 33 510.13 1.277 52 500.37 1.253 40 497.68 1.246 62 494.51 1.238 35 484.74 1.213 35 474.98 1.189 30 463.13 1.159 46 450.93 1.129 33 424.44 1.063 38 417.24 1.045 910 415.04 1.039 76 411.01 1.029 1000 401.37 1.005 48 398.93 0.999 50
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