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MassMS-NW-8741 2-methoxy-5-methylphenol C8H10O2 (Mass of molecular ion: 138)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.1 27.0 3.2 28.0 1.0 29.0 1.0 38.0 1.9 39.0 9.6 40.0 3.0 41.0 6.9 43.0 1.5 50.0 2.5 51.0 5.9 52.0 2.5 53.0 3.9 55.0 12.5 62.0 1.0 63.0 2.2 65.0 5.8 66.0 5.7 67.0 16.0 68.0 1.2 69.0 1.0 77.0 11.3 78.0 3.2 79.0 2.1 91.0 1.6 94.0 4.1 95.0 28.9 96.0 2.0 106.0 1.2 107.0 1.6 109.0 1.3 122.0 2.3 123.0 100.0 124.0 7.8 137.0 4.4 138.0 84.9 139.0 7.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 O2 0.042 g : 0.5 ml CDCl3 2-methoxy-5-methylphenol 
Assign. Shift(ppm)
A 6.752 B 6.726 C 6.630 D 5.63 E 3.825 F 2.247
Hz ppm Int.2699.34 6.755 133 2697.27 6.750 141 2692.99 6.739 139 2684.81 6.718 202 2654.54 6.643 80 2653.93 6.641 83 2652.47 6.637 77 2651.86 6.636 70 2646.48 6.622 54 2645.75 6.621 57 2644.41 6.617 53 2643.68 6.615 48 2248.90 5.628 108 1528.93 3.826 1000 898.32 2.248 670
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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