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1-BROMO-2,4-DICHLOROBENZENE

Product Name 1-BROMO-2,4-DICHLOROBENZENE

CAS1193-72-2

MFC6H3BrCl2

MW225.9

¹³CNMR

Mass

MS-NW-7683          
1-bromo-2,4-dichlorobenzene
C6H3BrCl2           (Mass of molecular ion:    224)

   Source Temperature: 270 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      36.0       1.6
      37.0       5.3
      38.0       2.5
      49.0       3.6
      50.0       8.2
      54.0       1.2
      54.5       2.5
      55.0       3.1
      60.0       1.0
      61.0       1.7
      62.0       1.2
      72.0       4.4
      72.5       1.3
      73.0       6.9
      74.0      22.6
      75.0      16.4
      76.0       1.0
      84.0       5.6
      85.0       2.7
      86.0       2.0
      94.0       1.9
      95.0       2.5
     108.0       1.8
     109.0      23.1
     110.0       9.0
     111.0       8.0
     112.0       5.3
     113.0       6.7
     114.0       3.0
     144.0       1.1
     145.0      45.5
     146.0       3.9
     147.0      30.0
     148.0       2.2
     149.0       4.9
     161.0       2.4
     163.0       1.4
     189.0       2.1
     191.0       2.5
     224.0      62.6
     225.0       4.3
     226.0     100.0
     227.0       6.8
     228.0      45.4
     229.0       3.3
     230.0       6.6

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₃ Br Cl₂	0.05 ml : 0.5 ml CDCl₃
1-bromo-2,4-dichlorobenzene

    Assign.     Shift(ppm)

      A             7.470
      B             7.405
      C             7.064

     Hz     ppm     Int.

    674.56   7.532    585
    674.31   7.530    585
    670.44   7.486     44
    665.75   7.434   1000
    664.38   7.419    796
    662.19   7.394    892
    658.38   7.352     56
    657.06   7.337     41
    637.31   7.117    681
    634.88   7.089    579
    631.69   7.054     48
    631.25   7.049     48
    628.75   7.021    456
    626.31   6.994    391
    622.75   6.954     30

in CDCl3

liquid film

4880 A,200 M,powder

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