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ALPHA-(CHLORODIMETHYLSILYL)CUMENE

Product Name ALPHA-(CHLORODIMETHYLSILYL)CUMENE

CAS118740-38-8

MFC11H17ClSi

MW212.79

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  • Mass 

    MS-IW-3602          
chloro(alpha,alpha-dimethylbenzyl)dimethylsilane
C11H17ClSi          (Mass of molecular ion:    212)


       Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV


          39.0       2.5
      41.0       8.5
      43.0       1.2
      51.0       2.3
      63.0       2.9
      65.0       5.0
      67.0       1.5
      73.0       2.6
      77.0       5.7
      78.0       3.6
      79.0       5.6
      91.0      32.8
      92.0       2.8
      93.0      32.0
      94.0       2.5
      95.0      11.4
     103.0       5.0
     104.0       1.1
     105.0       1.0
     115.0       2.0
     117.0       6.8
     118.0      52.7
     119.0     100.0
     120.0      10.1
     135.0       1.9
     155.0       2.7
     157.0       1.0
     177.0       1.1
     212.0      17.0
     213.0       2.9
     214.0       6.2
     215.0       1.0

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C11 H17 Cl Si 0.05 ml : 0.5 ml CDCl3
    chloro(alpha,alpha-dimethylbenzyl)dimethylsilane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.40
      B             7.39
      C             7.26
      D             1.577
      F             0.381
     
     CONFIRMED BY LAOCN PROGRAM.
  

         Hz     ppm     Int.


       2959.59   7.406    257
   2958.13   7.402    234
   2954.59   7.393    568
   2950.56   7.383     31
   2949.22   7.380     41
   2909.06   7.280     38
   2906.01   7.272     44
   2905.15   7.270     71
   2904.17   7.267     45
   2903.56   7.266     42
   2901.73   7.261     39
   2900.51   7.258     56
   2899.90   7.257     37
   2898.80   7.254     36
   2898.07   7.252     32
   2895.14   7.245     48
    633.54   1.586    123
    630.25   1.578    918
    626.71   1.569    112
    155.76   0.390    134
    152.47   0.382   1000
    149.05   0.373    123

in CDCl3



liquid film



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