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MassMS-NW-2313 3-phenylcarbamoyl-2-naphthyl acetate C19H15NO3 (Mass of molecular ion: 305)
Source Temperature: 240 °C Sample Temperature: 160 °C Direct, 75 eV
14.0 1.8 15.0 1.7 17.0 1.0 18.0 4.9 28.0 1.8 39.0 3.7 42.0 3.8 43.0 11.3 51.0 2.5 62.0 1.5 63.0 4.1 64.0 1.6 65.0 4.3 66.0 1.2 75.0 1.1 77.0 4.0 87.0 1.2 88.0 3.0 89.0 2.8 93.0 23.9 94.0 1.7 113.0 4.7 114.0 17.0 115.0 37.5 116.0 3.7 117.0 1.3 118.0 1.0 140.0 1.0 142.0 26.7 143.0 4.9 169.0 1.7 170.0 100.0 171.0 95.5 172.0 11.2 173.0 1.0 213.0 4.6 217.0 1.6 245.0 6.6 246.0 1.6 262.0 2.9 263.0 86.3 264.0 16.0 265.0 1.8 305.0 5.0 306.0 1.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C19 H15 N O3 0.040 g : 0.5 ml DMSO-d6 3-phenylcarbamoyl-2-naphthyl acetate 
Assign. Shift(ppm)
A 10.5 B 8.333 C 8.091 D 7.980 E 7.784 F 7.77 G *1 7.65 J *1 7.61 K 7.372 L 7.120 M 2.254
Hz ppm Int.4215.94 10.550 135 3330.52 8.334 210 3238.02 8.103 71 3230.14 8.083 78 3193.32 7.991 77 3185.45 7.971 85 3111.27 7.785 359 3102.47 7.763 141 3064.19 7.668 33 3062.73 7.664 41 3057.23 7.650 80 3055.95 7.647 78 3054.85 7.644 45 3049.54 7.631 88 3047.89 7.627 136 3046.24 7.623 91 3040.93 7.609 43 3039.83 7.607 74 3038.55 7.604 79 3033.05 7.590 37 3031.59 7.586 33 2954.11 7.392 113 2952.28 7.388 51 2949.90 7.382 30 2946.60 7.373 171 2942.57 7.363 42 2940.01 7.357 49 2938.36 7.353 122 2853.37 7.140 37 2852.27 7.137 68 2851.35 7.135 47 2844.94 7.119 110 2838.71 7.103 30 2837.62 7.101 50 2836.52 7.098 31 901.00 2.255 1000
in DMSO-d6
KBr disc
nujol mull
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