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4,4'-DICHLORODIPHENYL DISULFIDE

Product Name 4,4'-DICHLORODIPHENYL DISULFIDE

CAS1142-19-4

MFC12H8Cl2S2

MW287.23

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  • Mass 

    MS-KW-0490          
bis(p-chlorophenyl) disulfide
C12H8Cl2S2          (Mass of molecular ion:    286)


       Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV


          39.0       1.7
      45.0       2.0
      50.0       1.8
      51.0       1.3
      58.0       1.6
      62.0       1.3
      63.0       6.2
      69.0       5.4
      73.0       3.5
      74.0       1.2
      75.0       4.0
      81.0       1.2
      82.0       3.1
      99.0       8.6
     101.0       2.8
     107.0       2.6
     108.0      37.7
     109.0       4.3
     110.0       2.0
     111.0       1.6
     140.0       1.4
     142.0       1.9
     143.0     100.0
     144.0      10.5
     145.0      36.9
     146.0       3.6
     147.0       1.6
     175.0       1.2
     218.0       2.2
     222.0       5.3
     224.0       3.4
     251.0       1.0
     286.0      84.2
     287.0      13.2
     288.0      61.4
     289.0       9.4
     290.0      14.2
     291.0       2.0
     292.0       1.1

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H8 Cl2 S2 0.044 g : 0.5 ml CDCl3
    bis(p-chlorophenyl) disulfide
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.37
      B             7.26
  

         Hz     ppm     Int.


        668.88   7.469     33
    667.13   7.449    225
    666.44   7.442    178
    664.63   7.422    128
    663.38   7.408     28
    660.75   7.378    175
    658.25   7.350    953
    656.50   7.331    261
    654.44   7.308    220
    652.63   7.288   1000
    650.19   7.260    199
    647.81   7.234     32
    646.31   7.217    124
    644.50   7.197    164
    643.75   7.188    233
    642.06   7.170     42

in CDCl3



CCl4 solution



KBr disc



Nujol



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4,4'-DICHLORODIPHENYL DISULFIDE(1142-19-4)MS Atlas of Related Products

4,4'-DICHLORODIPHENYL DISULFIDE(1142-19-4)13CNMR 4,4'-DICHLORODIPHENYL DISULFIDE(1142-19-4)1HNMR 4,4'-DICHLORODIPHENYL DISULFIDE(1142-19-4)MS 4,4'-DICHLORODIPHENYL DISULFIDE(1142-19-4)IR1 4,4'-DICHLORODIPHENYL DISULFIDE(1142-19-4)IR2

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