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MS-NW-3759 3-aminobiphenyl-4-ol C12H11NO (Mass of molecular ion: 185)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
28.0 1.0 39.0 1.1 51.0 2.0 52.0 1.0 63.0 1.5 65.0 1.4 77.0 2.3 78.0 1.5 80.0 1.2 92.5 3.6 102.0 1.0 115.0 2.2 127.0 1.7 128.0 3.0 129.0 2.0 130.0 1.7 139.0 6.7 140.0 3.4 141.0 1.0 154.0 1.4 156.0 12.2 157.0 1.9 184.0 5.9 185.0 100.0 186.0 13.7 187.0 1.1
90 MHz in DMSO-d6
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1H NMR 89.56 MHz C12 H11 N O 0.042 g : 0.5 ml DMSO-d6 3-aminobiphenyl-4-ol Assign. Shift(ppm)
A 9. B 7.49 C 7.37 D 7.26 E 6.94 F 6.75 G 6.73 J 4.6
Hz ppm Int.
678.06 7.572 111 675.88 7.547 158 673.63 7.522 94 671.50 7.498 227 669.38 7.475 406 667.94 7.459 570 666.06 7.438 289 663.69 7.411 106 660.06 7.371 431 658.13 7.349 135 656.50 7.331 70 653.81 7.301 257 651.88 7.279 328 649.75 7.255 149 646.31 7.217 93 645.50 7.208 142 641.13 7.159 31 640.44 7.151 31 639.19 7.138 34 622.63 6.953 257 621.56 6.941 384 620.19 6.925 275 611.38 6.827 30 604.19 6.747 1000 603.25 6.736 653 414.31 4.627 44
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