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MassMS-NW-9653 trichloro(phenyl)stannane C6H5Cl3Sn (Mass of molecular ion: 302)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 1.8 27.0 1.4 28.0 1.4 35.0 1.1 36.0 2.3 38.0 1.6 39.0 4.4 50.0 10.5 51.0 23.8 52.0 8.3 57.0 3.2 63.0 2.3 74.0 4.2 75.0 3.4 76.0 8.1 77.0 54.5 78.0 61.4 79.0 4.1 112.0 100.0 113.0 7.1 114.0 33.1 115.0 3.8 116.0 3.5 117.0 2.2 118.0 6.1 119.0 2.7 120.0 8.3 122.0 1.1 124.0 1.4 126.0 1.2 127.0 1.3 128.0 1.8 143.0 1.5 145.0 2.0 147.0 1.4 149.0 1.5 150.0 1.3 151.0 16.2 152.0 15.6 153.0 32.1 154.0 69.2 155.0 44.7 156.0 8.4 157.0 16.9 158.0 6.5 159.0 8.4 161.0 2.1 186.0 2.0 187.0 1.1 188.0 4.7 189.0 2.0 190.0 6.8 191.0 1.0 192.0 3.8 193.0 1.5 194.0 2.1 195.0 2.4 196.0 1.5 197.0 3.8 198.0 1.0 199.0 3.2 201.0 2.1 228.0 2.7 229.0 1.7 230.0 5.3 231.0 2.5 232.0 7.6 233.0 1.2 234.0 3.2 236.0 1.8 263.0 5.4 264.0 3.1 265.0 12.3 266.0 5.7 267.0 18.3 268.0 3.9 269.0 10.8 270.0 1.2 271.0 4.7 273.0 1.9 298.0 2.1 299.0 1.2 300.0 5.3 301.0 2.7 302.0 8.4 303.0 2.1 304.0 6.2 305.0 3.2 306.0 4.7 307.0 5.7 308.0 4.3 309.0 7.5 310.0 2.2 311.0 3.8 313.0 2.2 342.0 1.7 344.0 2.8 346.0 2.3 348.0 1.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H5 Cl3 Sn 0.05 ml : 0.5 ml CDCl3 trichloro(phenyl)stannane 
Assign. Shift(ppm)
A 7.61 to 7.56
Hz ppm Int.3101.68 7.761 39 3099.24 7.755 38 3098.39 7.753 47 3096.07 7.747 48 3060.42 7.658 34 3056.40 7.648 57 3055.05 7.645 65 3052.25 7.638 115 3051.15 7.635 111 3049.93 7.632 151 3048.46 7.628 218 3046.14 7.623 278 3044.19 7.618 429 3042.60 7.614 251 3040.77 7.609 447 3038.33 7.603 631 3037.11 7.600 1000 3035.28 7.595 650 3034.42 7.593 438 3032.47 7.588 339 3031.13 7.585 779 3030.52 7.583 811 3025.63 7.571 402 3025.02 7.570 397 3023.19 7.565 270 3021.12 7.560 133 3018.19 7.553 122 3017.33 7.550 152 3015.01 7.545 91 3009.16 7.530 62 3007.08 7.525 63 3002.56 7.513 45 3001.22 7.510 61 3000.00 7.507 63 2993.90 7.492 35 2992.80 7.489 43 2986.82 7.474 40 2985.35 7.470 52 2984.25 7.468 54 2982.79 7.464 52
in CDCl3
liquid film
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