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1,2-Bis(2-chloroethoxy)ethane

Product Name 1,2-Bis(2-chloroethoxy)ethane

CAS112-26-5

MFC6H12Cl2O2

MW187.06

¹³CNMR

Mass

MS-NW-1221          
1,2-bis(2-chloroethoxy)ethane
C6H12Cl2O2          (Mass of molecular ion:    186)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       4.3
      19.0       1.1
      26.0       2.3
      27.0      41.4
      28.0       8.3
      29.0       5.6
      31.0       9.9
      43.0      18.1
      44.0       4.3
      45.0      26.0
      49.0       3.2
      51.0       1.0
      57.0       1.0
      58.0       1.0
      59.0       7.4
      62.0       3.4
      63.0     100.0
      64.0       3.2
      65.0      31.8
      72.0       2.8
      73.0      10.6
      93.0      48.9
      94.0       1.6
      95.0      15.3
     101.0       1.3
     106.0      12.6
     107.0      21.9
     108.0       5.0
     109.0       6.9
     137.0       4.8
     139.0       1.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₂ Cl₂ O₂	0.02 ml : 0.5 ml CDCl₃
1,2-bis(2-chloroethoxy)ethane

    Assign.     Shift(ppm)

      A             3.76
      B             3.694
      C             3.66

     Hz     ppm     Int.

    346.00   3.864     32
    343.00   3.830     55
    342.31   3.823     38
    337.94   3.774    181
    337.50   3.769    130
    334.25   3.733    180
    333.38   3.723    217
    330.81   3.694   1000
    329.50   3.680    230
    326.25   3.643    137
    325.81   3.638    188
    321.44   3.590     37
    320.69   3.581     57
    317.69   3.548     32

in CDCl3

CCl4 solution

liquid film

4880 A,200 M,liquid

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