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Tetrabutyl ammonium chloride

Product Name Tetrabutyl ammonium chloride

CAS1112-67-0

MFC16H36ClN

MW277.92

¹³CNMR

Mass

MS-NW-8201          
tetrabutylammonium chloride
C16H36ClN           (Mass of molecular ion:    277)

   Source Temperature: 180 °C
   Sample Temperature: 190 °C
   Direct, 75 eV

      26.0       1.1
      27.0       8.9
      28.0      20.7
      29.0      17.6
      30.0       6.8
      39.0       4.6
      41.0      24.5
      42.0       7.9
      43.0       8.2
      44.0      11.4
      55.0       4.9
      56.0      19.0
      57.0      15.5
      58.0       8.9
      70.0       1.7
      72.0       1.2
      84.0       3.2
      86.0       3.5
      98.0       3.7
     100.0      46.4
     101.0       3.4
     128.0       1.1
     142.0     100.0
     143.0      10.6
     184.0       1.2
     185.0       6.5
     186.0       1.1
     242.0       2.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₆ H₃₆ Cl N	0.046 g : 0.5 ml CDCl₃
tetrabutylammonium chloride

    Assign.     Shift(ppm)

      A             3.40
      B             1.67
      C             1.45
      D             1.02

     Hz     ppm     Int.

    328.63   3.670     33
    328.13   3.664     32
    306.06   3.418    274
    302.06   3.373    250
    301.19   3.363    250
    300.75   3.359    250
    300.31   3.354    250
    299.56   3.345    249
    297.56   3.323    255
    140.56   1.570    376
    135.13   1.509    308
    127.75   1.427    264
    121.06   1.352    173
    109.75   1.226     37
    109.31   1.221     36
    108.56   1.213     36
    107.56   1.201     34
    106.94   1.195     33
    106.25   1.187     33
    106.13   1.186     33
     96.25   1.075    581
     90.31   1.009   1000
     83.94   0.938    306

in CDCl3

CCl4 solution

KBr disc

liquid film

nujol mull

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