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MS-NW-8462 dibutylamine C8H19N (Mass of molecular ion: 129)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
18.0 1.4 27.0 6.1 28.0 6.2 29.0 20.7 30.0 61.9 31.0 1.0 39.0 3.5 41.0 17.6 42.0 4.6 43.0 5.3 44.0 72.0 45.0 1.9 55.0 3.1 56.0 4.4 57.0 17.3 58.0 1.4 70.0 1.5 72.0 2.5 84.0 1.7 86.0 100.0 87.0 5.9 128.0 1.5 129.0 7.1 130.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H19 N 0.04 ml : 0.5 ml CDCl3 dibutylamine Assign. Shift(ppm)
A 2.594 B 1.56 to 1.25 C 0.916
Hz ppm Int.
239.75 2.677 177 233.00 2.602 394 229.13 2.559 120 228.63 2.553 124 226.13 2.525 266 222.81 2.488 45 222.19 2.481 39 146.06 1.631 55 145.25 1.622 47 144.56 1.615 45 143.63 1.604 44 142.50 1.592 65 140.19 1.566 134 137.69 1.538 243 136.00 1.519 406 133.75 1.494 283 132.00 1.474 384 128.75 1.438 439 128.00 1.430 433 127.56 1.425 437 125.69 1.404 385 124.56 1.391 476 122.44 1.368 324 121.38 1.356 342 118.75 1.326 200 116.38 1.300 167 115.25 1.287 171 113.63 1.269 103 113.19 1.264 104 109.81 1.227 127 109.31 1.221 126 107.31 1.199 76 105.81 1.182 39 105.25 1.176 44 103.44 1.155 61 102.25 1.142 65 88.50 0.989 477 82.13 0.918 1000 79.69 0.890 305 78.25 0.874 247 76.19 0.851 180 74.69 0.834 200 72.81 0.813 108
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