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N,N,N',N'-TETRAMETHYL-1,4-BUTANEDIAMINE

Product Name N,N,N',N'-TETRAMETHYL-1,4-BUTANEDIAMINE

CAS111-51-3

MFC8H20N2

MW144.26

¹³CNMR

Mass

MS-NW-6432          
N,N,N',N'-tetramethyltetramethylenediamine
C8H20N2             (Mass of molecular ion:    144)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.3
      18.0       1.4
      27.0       1.2
      28.0       1.6
      29.0       1.7
      30.0       3.1
      41.0       1.6
      42.0       9.5
      43.0       3.2
      44.0       5.5
      45.0      22.3
      55.0       1.5
      56.0       3.1
      57.0       1.8
      58.0     100.0
      59.0       3.8
      70.0       1.4
      71.0      17.2
      72.0       6.2
      73.0       3.1
      84.0       9.6
      85.0       1.8
      86.0       1.0
      98.0       5.6
      99.0       1.7
     100.0       4.2
     101.0       1.4
     129.0       4.6
     144.0       8.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₂₀ N₂	0.05 ml : 0.5 ml CDCl₃
N,N,N',N'-tetramethyltetramethylenediamine

    Assign.     Shift(ppm)

      A             2.261
      B             2.210
      C             1.476

     Hz     ppm     Int.

    911.74   2.282    107
    910.52   2.279     97
    908.94   2.275    102
    904.54   2.264    170
    900.02   2.253    102
    898.44   2.249    109
    897.34   2.246    130
    896.36   2.243    105
    883.18   2.210   1000
    597.17   1.495    105
    593.63   1.486    112
    591.92   1.482     98
    589.84   1.476    214
    585.82   1.466    122
    582.64   1.458    109

in CDCl3

liquid film

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