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N-METHYLBUTYLAMINE

Product Name N-METHYLBUTYLAMINE

CAS110-68-9

MFC5H13N

MW87.16

¹³CNMR

Mass

MS-NW-2184          
N-methylbutylamine
C5H13N              (Mass of molecular ion:     87)

   Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.6
      18.0       1.7
      27.0       2.9
      28.0       3.3
      29.0       2.7
      30.0       4.5
      39.0       1.5
      41.0       2.6
      42.0       3.8
      43.0       2.1
      44.0     100.0
      45.0       2.7
      56.0       1.3
      57.0       1.5
      58.0       3.7
      87.0       6.7

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₅ H₁₃ N	0.04 ml : 0.5 ml CDCl₃
N-methylbutylamine

    Assign.     Shift(ppm)

      A             2.56
      B             2.429
      C          1.69 to 1.10
      D             1.38
      E             0.92

     Hz     ppm     Int.

    237.38   2.651     37
    236.81   2.645     35
    230.06   2.569     96
    223.31   2.494     61
    217.50   2.429   1000
    133.06   1.486     37
    132.06   1.475     54
    131.44   1.468     51
    129.00   1.441     71
    127.94   1.429     80
    125.75   1.405     65
    123.50   1.379    329
    121.50   1.357     74
    119.38   1.333     37
    118.44   1.323     33
    115.56   1.291     30
     89.75   1.003     50
     88.75   0.991     76
     86.63   0.968     40
     84.94   0.949     33
     82.44   0.921    177
     79.88   0.892     47
     79.38   0.887     48
     75.00   0.838     35

in CDCl3

CCl4 solution

liquid film

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