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MS-NW-0019 2-methyl-1-(vinyloxy)propane C6H12O (Mass of molecular ion: 100)
Source Temperature: 203 °C Sample Temperature: 65 °C Reservoir, 75 eV
14.0 1.2 15.0 5.6 26.0 3.5 27.0 24.6 28.0 4.8 29.0 57.1 30.0 1.3 31.0 11.4 38.0 2.1 39.0 23.1 40.0 3.3 41.0 100.0 42.0 6.0 43.0 9.2 44.0 18.5 45.0 4.8 51.0 1.1 53.0 2.2 55.0 12.2 56.0 69.8 57.0 99.7 58.0 4.9 59.0 4.5 67.0 1.3 73.0 1.2 85.0 1.3 100.0 20.9 101.0 1.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H12 O 0.04 ml : 0.5 ml CDCl3 2-methyl-1-(vinyloxy)propane Assign. Shift(ppm)
A 6.470 B 4.159 C 3.953 D 3.441 E 1.94 F 0.95
Hz ppm Int.
590.50 6.594 67 583.69 6.518 71 576.19 6.434 75 569.38 6.358 79 380.19 4.246 94 378.31 4.225 106 365.88 4.086 76 364.06 4.065 101 358.19 4.000 123 356.38 3.980 108 351.38 3.924 125 349.56 3.904 95 311.63 3.480 247 305.13 3.407 272 181.38 2.026 39 174.50 1.949 50 167.88 1.875 47 161.38 1.802 31 87.94 0.982 1000 84.25 0.941 33 81.44 0.910 765
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