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MassMS-NW-0773 2-methylpyridine C6H7N (Mass of molecular ion: 93)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 2.4 27.0 3.2 28.0 2.8 37.0 2.5 38.0 4.6 39.0 14.2 40.0 6.3 41.0 2.4 42.0 1.6 46.5 2.3 50.0 5.6 51.0 11.5 52.0 6.4 53.0 4.3 54.0 1.7 61.0 1.2 62.0 1.8 63.0 4.3 64.0 2.5 65.0 14.0 66.0 39.9 67.0 7.9 78.0 15.9 79.0 1.0 91.0 1.3 92.0 20.4 93.0 100.0 94.0 7.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H7 N 0.04 ml : 0.5 ml CDCl3 2-methylpyridine 
Assign. Shift(ppm)
A 8.477 B 7.538 C 7.12 D 7.08 E 2.547 J(A,B)=1.8HZ, J(A,D)=4.8HZ, J(B,C)=7.9HZ, J(B,D)=7.4HZ
Hz ppm Int.761.56 8.504 69 757.38 8.457 72 756.88 8.452 73 685.06 7.650 41 683.25 7.629 42 677.63 7.567 79 675.63 7.544 95 669.88 7.480 88 668.00 7.459 85 642.19 7.171 129 639.25 7.138 85 638.81 7.133 83 634.38 7.084 141 633.94 7.079 141 631.50 7.052 68 627.06 7.002 46 626.56 6.996 50 625.88 6.989 46 228.19 2.548 1000
in CDCl3
CCl4 solution
KBr disc
liquid film
X-IRRAD. OF ADAMANTANE RECRYST. FROM 2-PICOLINE
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