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2-Amino-5-methyl-1,3,4-thiadiazole

Product Name 2-Amino-5-methyl-1,3,4-thiadiazole

CAS108-33-8

MFC3H5N3S

MW115.16

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  • Mass 

    MS-NW-4948          
5-methyl-1,3,4-thiadiazol-2-amine
C3H5N3S             (Mass of molecular ion:    115)


       Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          13.0       1.0
      14.0       1.2
      15.0       3.2
      18.0       2.1
      26.0       4.0
      27.0       6.2
      28.0      12.6
      29.0       2.7
      30.0       1.0
      32.0       2.4
      33.0       1.8
      36.0       1.5
      39.0       1.4
      40.0       3.4
      41.0       5.2
      42.0      12.4
      43.0       2.8
      44.0       2.1
      45.0       5.8
      46.0       3.1
      47.0       9.6
      56.0       5.3
      57.0       2.2
      58.0       6.7
      59.0      26.5
      60.0      16.1
      61.0       1.7
      72.0       4.6
      73.0       5.0
      74.0     100.0
      75.0       3.2
      76.0       4.6
     115.0      50.7
     116.0       2.9
     117.0       2.4

parameter in CDCl3


  • 1H NMR 300 MHz
    C3 H5 N3 S 0.052 g : 0.5 ml DMSO-d6
    5-methyl-1,3,4-thiadiazol-2-amine
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         7.00
     
      D(B)         2.443
  

         Hz     ppm     Int.


       2100.00   7.000    113
    732.89   2.443   1000

in DMSO-d6



KBr disc



nujol mull



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