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1,3-Dibromobutane

Product Name 1,3-Dibromobutane

CAS107-80-2

MFC4H8Br2

MW215.91

¹³CNMR

Mass

MS-NW-4384          
1,3-dibromobutane
C4H8Br2             (Mass of molecular ion:    214)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      26.0       4.2
      27.0      30.7
      28.0       1.0
      29.0      28.1
      38.0       1.5
      39.0      14.3
      40.0       1.3
      41.0       9.9
      42.0       1.1
      50.0       1.6
      51.0       1.7
      53.0       5.8
      54.0       1.4
      55.0     100.0
      56.0       5.2
      79.0       1.0
      80.0       1.0
      81.0       1.0
      82.0       1.1
      93.0       2.1
      95.0       2.0
     107.0       7.0
     109.0       6.5
     119.0       1.1
     121.0       1.4
     134.0       1.9
     135.0      59.4
     136.0       4.6
     137.0      57.2
     138.0       2.7
     214.0       1.3
     216.0       2.5
     218.0       1.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₄ H₈ Br₂	0.02 ml : 0.5 ml CDCl₃
1,3-dibromobutane

    Assign.     Shift(ppm)

      A             4.31
      B             3.552
      C             2.27
      D             1.757

     Hz     ppm     Int.

    324.94   3.629    196
    319.13   3.564    356
    318.19   3.553    226
    317.56   3.546    234
    311.94   3.484    261
    208.00   2.323    112
    206.25   2.303    165
    204.94   2.289    146
    200.19   2.236    116
    199.44   2.227    165
    160.69   1.795   1000
    154.00   1.720    939

in CDCl3

liquid film

4880 A,200 M,liquid

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