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1,4-Dichlorobenzene

Product Name 1,4-Dichlorobenzene

CAS106-46-7

MFC6H4Cl2

MW147

¹³CNMR

Mass

MS-NW-1381          
p-dichlorobenzene
C6H4Cl2             (Mass of molecular ion:    146)

   Source Temperature: 250 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      36.0       1.0
      37.0       4.1
      37.5       1.3
      38.0       3.4
      49.0       2.8
      50.0      14.2
      51.0       4.9
      55.0       4.6
      56.0       1.5
      61.0       1.5
      73.0       7.5
      74.0      12.0
      75.0      24.2
      76.0       3.3
      84.0       2.2
      85.0       3.1
      86.0       1.4
     109.0       1.3
     110.0       2.8
     111.0      34.3
     112.0       3.0
     113.0      10.9
     146.0     100.0
     147.0       7.0
     148.0      65.4
     149.0       4.4
     150.0      10.5

parameter neat

parameter in CDCl3

parameter in cyclohexane

¹H NMR	300 MHz
C₆ H₄ Cl₂	neat
p-dichlorobenzene

    Parameter     ppm  Hz

      D(A)         7.070
     
     CRECELY,R.W. ET AL. SPECTROCHIM.ACTA 24A, 685 (1968)

     Hz     ppm     Int.

   2121.00   7.070   1000

¹H NMR	300 MHz
C₆ H₄ Cl₂	0.045 g : 0.5 ml CDCl₃
p-dichlorobenzene

    Parameter     ppm  Hz

      D(A)         7.255

     Hz     ppm     Int.

   2176.50   7.255   1000

¹H NMR	300 MHz
C₆ H₄ Cl₂	in cyclohexane
p-dichlorobenzene

    Parameter     ppm  Hz

      D(A)         7.201
     
     MARTIN,J. & DAILEY,B.P. J.CHEM.PHYS. 37, 2594 (1962)

     Hz     ppm     Int.

   2160.30   7.201   1000

in CDCl3

CCl4 solution

KBr disc

nujol mull

4880 A,100M,powder

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