-
MS-NW-5055 (+-)-3-amino-2-methylpropionic acid C4H9NO2 H2O (Mass of molecular ion: 103)
Source Temperature: 170 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 2.4 27.0 2.6 28.0 7.6 29.0 2.1 30.0 100.0 31.0 1.7 39.0 1.5 41.0 2.9 42.0 2.1 45.0 1.6 55.0 1.1 56.0 3.8 57.0 1.7 73.0 1.4 74.0 1.2 84.0 1.1 103.0 1.9
90 MHz in D2O
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1H NMR 89.56 MHz C4 H9 N O2 0.046 g : 0.5 ml D2O (+-)-3-amino-2-methylpropionic acid Assign. Shift(ppm)
A *1 3.12 B *1 3.03 C 2.61 D 1.198 SOLVENT PEAK REMOVED
Hz ppm Int.
292.75 3.269 33 284.69 3.179 30 280.13 3.128 312 277.25 3.096 292 271.75 3.035 620 264.56 2.954 36 110.44 1.234 1000 107.69 1.203 45 107.38 1.199 43 103.31 1.154 855
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