1-ALLYL-3-(2-HYDROXYETHYL)-2-THIOUREA

Mass

MS-NW-0208          
1-allyl-3-(2-hydroxyethyl)thiourea
C6H12N2OS           (Mass of molecular ion:    160)

   Source Temperature: 220 °C
   Sample Temperature:   0 °C
   Direct, 75 eV

      15.0       5.7
      18.0       3.6
      19.0       2.9
      26.0       2.2
      27.0      12.6
      28.0      31.5
      29.0       4.8
      30.0      59.1
      31.0       6.9
      32.0       1.4
      33.0       1.1
      34.0       1.8
      38.0       2.2
      39.0      31.7
      40.0       3.2
      41.0     100.0
      42.0      15.8
      43.0      28.5
      44.0      15.6
      45.0      18.3
      46.0       2.1
      47.0       2.2
      52.0       1.2
      54.0       7.8
      55.0       8.4
      56.0      74.3
      57.0      50.7
      58.0      11.0
      59.0       8.5
      60.0      30.0
      61.0       3.1
      62.0       7.0
      67.0       2.7
      68.0       3.7
      69.0       7.1
      70.0       2.6
      71.0       2.4
      72.0       7.4
      73.0       8.5
      74.0       8.8
      75.0       2.5
      76.0       1.0
      77.0       4.2
      81.0       2.2
      82.0       2.2
      83.0      17.8
      84.0       2.3
      85.0       1.5
      86.0      17.3
      87.0       3.2
      88.0       2.0
      90.0       1.5
      95.0       2.1
      98.0       2.0
      99.0       3.5
     100.0       9.9
     101.0      32.5
     102.0       2.4
     103.0       3.2
     104.0       3.5
     109.0       1.1
     113.0       2.5
     114.0       3.3
     115.0      12.6
     116.0       3.2
     117.0       3.2
     125.0       2.2
     126.0       2.0
     127.0       8.4
     129.0       3.8
     131.0       1.0
     141.0       4.0
     142.0       5.0
     143.0       1.8
     145.0      80.1
     146.0       5.7
     147.0       4.1
     159.0       3.4
     160.0      97.2
     161.0       9.1
     162.0       5.1

Assign. Shift(ppm) A *1 7.60 B *1 7.44 C 5.837 D 5.146 E 5.071 F 4.77 G 4.05 J 3.48 SIGNAL J OVERLAPPED BY THE IMPURITY PEAK.

     Hz     ppm     Int.

   3038.82   7.604    184
   2974.37   7.443    243
   2348.63   5.877    166
   2343.63   5.865    173
   2338.26   5.851    213
   2337.16   5.849    179
   2331.54   5.834    241
   2326.29   5.821    210
   2321.17   5.809    221
   2065.92   5.170    394
   2064.33   5.166    434
   2062.62   5.162    256
   2048.71   5.127    376
   2047.12   5.123    421
   2045.53   5.119    265
   2032.59   5.086    432
   2031.01   5.082    456
   2022.34   5.061    401
   2020.75   5.057    412
   1907.96   4.775    203
   1617.92   4.049    372
   1394.29   3.489    760
   1389.40   3.477   1000
   1367.80   3.423    219