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4-METHYL-2-PENTANONE OXIME

Product Name 4-METHYL-2-PENTANONE OXIME

CAS105-44-2

MFC6H13NO

MW115.17

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  • Mass 

    MS-NW-1209          
4-methyl-2-pentanone oxime
C6H13NO             (Mass of molecular ion:    115)


       Source Temperature: 240 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          15.0       5.4
      18.0       3.6
      27.0      11.4
      28.0       7.7
      29.0       8.6
      30.0       1.7
      31.0       2.4
      32.0       1.2
      33.0       4.3
      38.0       1.2
      39.0      11.5
      40.0       3.0
      41.0      30.3
      42.0      35.3
      43.0      20.0
      44.0       1.1
      45.0       1.5
      53.0       1.4
      54.0       7.3
      55.0       7.1
      56.0      11.1
      57.0      18.7
      58.0       5.2
      60.0       1.9
      69.0       2.9
      72.0       1.0
      73.0     100.0
      74.0       4.2
      82.0       2.1
      83.0       3.7
      84.0       3.1
      97.0       1.0
      98.0       2.5
     100.0      12.3
     115.0       2.4

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H13 N O 0.04 ml : 0.5 ml CDCl3
    4-methyl-2-pentanone oxime
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             9.6
      B     *1      2.27
      C             2.06
      D     *1      2.05
      E     *2      1.874
      F     *2      1.865
      G     *3      0.942
      J     *3      0.916
  

         Hz     ppm     Int.


        207.81   2.321     28
    201.54   2.251     65
    189.72   2.119     33
    187.81   2.098     59
    184.24   2.058     72
    182.26   2.036    183
    176.70   1.973     25
    175.75   1.963     28
    167.82   1.874   1000
    167.02   1.865    379
    164.88   1.842     28
    163.61   1.827     24
     87.60   0.979    197
     84.82   0.948    492
     81.25   0.908    219
     78.47   0.877    392

in CDCl3



CCl4 solution



liquid film



4880 A,200 M,liquid



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