CROTONYL CHLORIDE

Mass

MS-NW-2640          
crotonoyl chloride
C4H5ClO             (Mass of molecular ion:    104)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       2.3
      26.0       3.5
      27.0       3.0
      28.0       1.7
      35.0       1.0
      36.0       2.5
      37.0       5.0
      38.0       8.0
      39.0      53.6
      40.0       7.7
      41.0      57.8
      42.0       2.4
      53.0       1.0
      63.0       1.7
      68.0       2.5
      69.0     100.0
      70.0       4.4
      76.0       1.9
      77.0       1.4
     105.0       1.9

Assign. Shift(ppm) A 7.24 B 6.11 C 1.997

     Hz     ppm     Int.

    667.31   7.451     62
    660.31   7.373    193
    653.38   7.296    206
    652.25   7.283     89
    646.50   7.219     70
    645.25   7.205    257
    638.31   7.128    261
    631.44   7.051     88
    555.81   6.207     98
    554.19   6.188    285
    552.56   6.170    284
    550.94   6.152     93
    540.75   6.038     63
    539.06   6.019    206
    537.44   6.001    215
    535.81   5.983     71
    183.13   2.045    982
    181.50   2.027    990
    179.69   2.007     48
    176.19   1.968    957
    174.56   1.950   1000
    172.13   1.922     33