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MassMS-NW-5855 p-methylbenzylamine C8H11N (Mass of molecular ion: 121)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 4.1 28.0 20.3 29.0 3.9 30.0 26.3 38.0 2.0 39.0 10.1 40.0 1.2 41.0 3.1 42.0 1.0 46.0 1.2 50.0 3.8 51.0 7.9 52.0 2.8 53.0 2.8 54.0 1.2 58.0 2.1 59.5 7.9 60.0 1.1 62.0 2.2 63.0 5.7 64.0 1.6 65.0 10.8 66.0 1.5 74.0 1.1 76.0 1.1 77.0 23.9 78.0 6.4 79.0 16.0 80.0 1.9 89.0 3.4 90.0 1.8 91.0 31.2 92.0 7.8 93.0 35.6 94.0 3.1 102.0 1.1 103.0 6.5 104.0 100.0 105.0 29.1 106.0 54.0 107.0 5.8 117.0 1.4 118.0 4.4 119.0 2.8 120.0 77.5 121.0 34.0 122.0 4.2 223.0 1.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 0.04 ml : 0.5 ml CDCl3 p-methylbenzylamine 
Assign. Shift(ppm)
A 7.32 to 6.96 B 3.795 C 2.320 D 1.42
Hz ppm Int.649.25 7.250 27 648.06 7.237 23 640.38 7.151 735 636.69 7.110 31 631.38 7.050 24 631.00 7.046 25 339.88 3.795 459 207.81 2.321 745 126.69 1.415 1000
in CDCl3
liquid film
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