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MassMS-NW-1016 decylbenzene C16H26 (Mass of molecular ion: 218)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
18.0 1.0 27.0 3.5 29.0 6.0 39.0 3.2 41.0 10.0 42.0 1.9 43.0 15.9 51.0 1.3 55.0 4.7 56.0 1.7 57.0 7.4 65.0 3.9 69.0 1.4 70.0 1.2 71.0 4.9 77.0 2.7 78.0 4.3 79.0 2.5 82.0 1.7 83.0 2.5 85.0 2.5 91.0 63.6 92.0 100.0 93.0 7.8 103.0 1.2 104.0 4.0 105.0 8.8 106.0 1.9 117.0 1.7 119.0 2.5 120.0 1.6 121.0 1.4 133.0 6.6 134.0 2.0 147.0 1.0 218.0 19.1 219.0 3.3
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C16 H26 15.2 mg : 0.5 ml CDCl3 decylbenzene 
Assign. Shift(ppm)
A 7.27 B 7.18 C 7.18 D 2.596 E 1.604 F 1.30 G 1.26 J 0.878
Hz ppm Int.2913.57 7.291 117 2911.87 7.287 50 2908.20 7.277 79 2906.25 7.272 210 2905.27 7.270 247 2902.71 7.264 34 2901.37 7.260 65 2898.68 7.254 246 2896.12 7.247 187 2872.07 7.187 449 2869.38 7.180 88 2864.75 7.169 321 2858.76 7.154 52 2857.54 7.151 63 1045.41 2.616 159 1037.60 2.597 191 1029.91 2.578 174 651.00 1.629 52 649.54 1.626 67 648.56 1.623 61 647.71 1.621 58 645.63 1.616 55 642.21 1.607 100 639.89 1.602 71 638.18 1.597 58 637.45 1.596 58 636.84 1.594 65 634.52 1.588 81 627.69 1.571 34 627.08 1.570 37 538.45 1.348 41 537.48 1.345 50 536.74 1.344 55 536.38 1.343 57 535.64 1.341 60 534.79 1.339 62 534.06 1.337 65 531.25 1.330 100 524.66 1.313 204 524.05 1.312 203 523.68 1.311 203 520.51 1.303 273 518.80 1.299 246 515.01 1.289 183 513.06 1.284 198 512.45 1.283 198 510.62 1.278 219 502.69 1.258 1000 490.23 1.227 70 489.87 1.226 67 488.28 1.222 58 487.79 1.221 56 486.21 1.217 43 485.23 1.215 38 484.50 1.213 35 357.79 0.896 190 351.20 0.879 576 348.75 0.873 86 344.12 0.862 230
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1H NMR 89.56 MHz C16 H26 0.04 ml : 0.5 ml CDCl3 decylbenzene Assign. Shift(ppm)
A 7.47 to 6.98 B 2.58 C 1.60 D 1.26 E 0.88
Hz ppm Int.654.56 7.309 31 652.69 7.288 42 650.06 7.259 79 647.75 7.233 68 645.50 7.208 429 644.13 7.193 440 640.38 7.151 61 637.94 7.124 43 636.63 7.109 42 239.88 2.679 50 233.06 2.603 99 225.00 2.513 92 145.31 1.623 33 145.06 1.620 33 144.81 1.617 33 142.50 1.592 38 142.31 1.589 38 139.81 1.562 30 135.88 1.518 34 112.88 1.261 1000 83.75 0.936 72 81.00 0.905 57 78.63 0.878 217 74.31 0.830 34 72.56 0.811 50
in CDCl3
liquid film
4880 A,200 M,liquid
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