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MassMS-IW-1524 5,6-epoxy-1-hexene C6H10O (Mass of molecular ion: 98)
Source Temperature: 250 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 4.8 26.0 4.1 27.0 43.8 28.0 9.0 29.0 52.7 30.0 1.3 31.0 63.7 37.0 2.2 38.0 6.0 39.0 72.0 40.0 22.7 41.0 87.1 42.0 38.2 43.0 18.0 44.0 12.1 45.0 2.0 50.0 3.6 51.0 5.1 52.0 3.2 53.0 38.8 54.0 91.0 55.0 68.8 56.0 13.8 57.0 42.1 58.0 3.1 62.0 1.0 63.0 1.6 65.0 11.0 66.0 5.6 67.0 100.0 68.0 49.8 69.0 26.7 70.0 11.4 71.0 4.4 77.0 1.8 79.0 12.7 80.0 7.8 81.0 2.4 83.0 15.9 97.0 6.9 147.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H10 O 0.05 ml : 0.5 ml CDCl3 5,6-epoxy-1-hexene 
Assign. Shift(ppm)
A 5.841 B 5.062 C 4.990 D 2.927 E 2.741 F 2.474 G 2.220 J 1.631 J(A,B)=17.0HZ J(A,C)=10.1HZ J(A,G)=6.7HZ J(D,E)=3.6HZ J(D,F)=2.8HZ J(E,F)=-5.2HZ
Hz ppm Int.2355.22 5.894 198 2348.51 5.877 386 2345.09 5.868 221 2342.04 5.861 218 2338.26 5.851 560 2331.54 5.834 579 2327.88 5.825 238 2324.83 5.818 233 2321.29 5.809 441 2314.70 5.792 231 2033.57 5.089 352 2031.98 5.085 717 2030.03 5.080 793 2028.44 5.076 364 2016.48 5.046 324 2014.89 5.042 650 2012.94 5.037 745 2011.35 5.033 342 2001.34 5.008 364 2000.12 5.005 681 1999.51 5.004 551 1998.90 5.002 532 1998.17 5.000 639 1996.95 4.997 335 1991.21 4.983 333 1989.99 4.980 617 1989.38 4.978 521 1988.77 4.977 495 1988.04 4.975 625 1986.82 4.972 320 1178.71 2.950 224 1176.03 2.943 256 1174.80 2.940 297 1173.58 2.937 294 1172.24 2.934 407 1170.78 2.930 317 1169.68 2.927 470 1168.95 2.925 361 1166.87 2.920 393 1166.26 2.919 334 1164.79 2.915 282 1163.45 2.912 282 1160.77 2.905 251 1099.73 2.752 861 1095.83 2.742 862 1094.73 2.740 1000 1090.70 2.730 810 992.68 2.484 910 989.87 2.477 860 987.55 2.472 806 984.86 2.465 774 915.77 2.292 42 914.31 2.288 34 910.16 2.278 52 908.94 2.275 89 907.71 2.272 77 905.15 2.265 42 902.47 2.259 182 901.12 2.255 254 899.78 2.252 177 896.97 2.245 186 895.75 2.242 398 894.41 2.238 543 893.19 2.235 433 891.72 2.232 229 888.67 2.224 561 887.45 2.221 654 886.23 2.218 543 883.06 2.210 212 881.84 2.207 442 880.49 2.204 563 879.27 2.201 440 875.12 2.190 177 873.78 2.187 262 872.44 2.184 185 868.41 2.173 48 867.19 2.170 77 865.97 2.167 95 864.75 2.164 62 860.47 2.154 37 859.13 2.150 49 857.79 2.147 36 678.10 1.697 72 672.97 1.684 89 671.02 1.680 90 669.80 1.676 69 665.89 1.667 131 664.18 1.662 425 659.18 1.650 597 656.25 1.643 507 652.95 1.634 581 651.73 1.631 707 648.93 1.624 414 646.00 1.617 501 643.92 1.612 514 638.43 1.598 337 632.81 1.584 66 631.35 1.580 98 624.51 1.563 56
in CDCl3
liquid film
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