SpectrumDetail Supplier Related Products
WebSite > CAS DataBase List >  1034-49-7More Spectrum > (BROMOMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE(1034-49-7)MS

1034-49-7

(BROMOMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE

Product Name (BROMOMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE

CAS1034-49-7

MFC19H17Br2P

MW436.12

More

  • 1034-49-7_ms
    Mass

    MS-NW-7000          
    (bromomethyl)triphenylphosphonium bromide
    C19H17Br2P          (Mass of molecular ion:    434)
    

       Source Temperature: 250 °C
       Sample Temperature: 280 °C
       Direct, 75 eV
    

          15.0       1.7
          39.0       2.6
          50.0       2.0
          51.0       7.1
          57.0       3.0
          63.0       1.9
          65.0       1.8
          77.0       3.7
          78.0       1.3
          79.0       5.1
          80.0      10.9
          81.0       4.9
          82.0      10.6
          83.0       1.4
          89.0       1.0
          91.0       1.5
          93.0       1.6
          94.0       5.4
          95.0       1.3
          96.0       5.2
         107.0      15.0
         108.0      34.7
         109.0       3.4
         115.0       3.9
         128.0       1.4
         131.0       1.9
         133.0       3.4
         139.0       1.8
         141.0       1.7
         152.0       8.4
         153.0       2.1
         154.0       2.2
         157.0       4.2
         165.0       1.2
         170.0       3.0
         181.0       1.5
         183.0      70.4
         184.0      15.0
         185.0      13.3
         186.0       1.9
         259.0       1.1
         260.0       1.4
         261.0      17.5
         262.0     100.0
         263.0      20.3
         264.0       2.3
         275.0       8.8
         276.0       3.5
         277.0       2.5
    

400 MHz in D2O at 60.C

400 MHz in DMSO-d6

  • 1034-49-7_1hnmr_2

    1H NMR 399.65 MHz
    C19 H17 Br2 P 0.031 g : 0.5 ml D2O at 60 C
    (bromomethyl)triphenylphosphonium bromide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.986 B 7.867 C 7.813 D 2.919

         Hz     ppm     Int.
    

       3200.44   8.009    214
       3199.22   8.006    182
       3198.36   8.003    223
       3196.90   8.000    147
       3194.82   7.995    162
       3192.99   7.990    547
       3192.02   7.988    348
       3191.04   7.985    551
       3189.33   7.981    214
       3186.89   7.975    173
       3185.30   7.971    354
       3183.72   7.967    339
       3182.13   7.963    173
       3156.86   7.900    427
       3155.76   7.897    543
       3150.63   7.884    269
       3148.56   7.879    945
       3147.22   7.875    812
       3144.17   7.868    363
       3142.82   7.864    497
       3141.24   7.860    263
       3137.94   7.852    265
       3135.74   7.847   1000
       3134.28   7.843    869
       3129.39   7.831    720
       3127.44   7.826    317
       3125.37   7.821    779
       3121.95   7.812    801
       3118.04   7.802    814
       3115.72   7.797    326
       3113.77   7.792    354
       3111.57   7.786    206
       3109.50   7.781    306
       3108.52   7.779    333
       3104.00   7.767    221
       3096.56   7.749    155
       1173.46   2.937    114
       1159.55   2.902    114
    

  • 1034-49-7_1hnmr

    1H NMR 399.65 MHz
    C19 H17 Br2 P 0.036 g : 0.5 ml DMSO-d6
    (bromomethyl)triphenylphosphonium bromide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.963 B 7.904 C 7.825 D 5.813

         Hz     ppm     Int.
    

       3192.02   7.988    215
       3190.31   7.983    207
       3188.72   7.979    132
       3184.69   7.969    549
       3182.86   7.965    555
       3177.12   7.950    377
       3175.78   7.947    392
       3173.95   7.942    283
       3171.26   7.936    593
       3164.06   7.918    989
       3162.60   7.914    710
       3159.42   7.906    494
       3158.45   7.904    558
       3151.25   7.886   1000
       3149.78   7.882    730
       3138.67   7.854    662
       3134.89   7.845    725
       3130.98   7.835    805
       3127.32   7.826    805
       3123.05   7.815    373
       3120.97   7.810    194
       3119.14   7.805    376
       3116.70   7.799    148
       3114.01   7.792     33
       3113.65   7.791     34
       3112.55   7.789     30
       3109.38   7.781    219
       3104.86   7.769    154
       2326.66   5.822    540
       2319.70   5.805    533
    

in DMSO-d6

  • 1034-49-7_13cnmr

KBr disc

  • 1034-49-7_ir1_2

nujol mull

  • 1034-49-7_ir2

  • 1034-49-7_raman