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MassMS-NW-6837 di(p-tolyl) disulfide C14H14S2 (Mass of molecular ion: 246)
Source Temperature: 270 °C Sample Temperature: 200 °C Reservoir, 75 eV
27.0 1.6 28.0 1.7 39.0 6.4 41.0 1.0 45.0 17.2 50.0 1.2 51.0 3.6 52.0 1.2 53.0 2.3 62.0 1.1 63.0 3.2 65.0 4.3 69.0 4.0 70.0 1.1 71.0 1.6 77.0 12.4 78.0 4.5 79.0 14.8 80.0 1.3 82.0 1.0 89.0 2.3 90.0 1.1 91.0 14.8 92.0 1.7 95.0 1.0 97.0 2.2 108.0 3.6 121.0 6.5 122.0 6.4 123.0 89.8 124.0 19.6 125.0 5.2 154.0 2.0 167.0 1.3 181.0 1.0 182.0 5.2 198.0 2.0 199.0 1.0 213.0 2.4 214.0 4.7 246.0 100.0 247.0 17.4 248.0 10.8 249.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H14 S2 0.038 g : 0.5 ml CDCl3 di(p-tolyl) disulfide 
Assign. Shift(ppm)
A 7.371 B 7.088 C 2.300
Hz ppm Int.2952.76 7.389 62 2950.56 7.383 356 2948.85 7.379 141 2944.34 7.368 142 2942.38 7.363 419 2836.30 7.097 282 2835.69 7.096 311 2827.76 7.076 281 919.19 2.300 1000
in CDCl3
KBr disc
nujol mull
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