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MS-NW-5536 2,2',2''-nitrilotriethanol C6H15NO3 (Mass of molecular ion: 149)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 4.0 17.0 1.0 18.0 4.0 19.0 2.2 26.0 1.2 27.0 6.4 29.0 3.4 30.0 15.0 31.0 3.5 41.0 3.3 42.0 13.4 43.0 4.9 44.0 8.2 45.0 23.4 54.0 1.3 55.0 1.4 56.0 36.5 57.0 3.2 58.0 2.5 70.0 2.9 72.0 1.5 73.0 1.1 74.0 37.6 75.0 2.2 86.0 2.4 88.0 2.9 100.0 2.8 104.0 1.5 116.0 1.4 118.0 100.0 119.0 6.1 126.0 1.0 129.0 1.6 130.0 2.0 174.0 4.6
90 MHz in CDCl3
in CDCl3
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1H NMR 89.56 MHz C6 H15 N O3 0.04 ml : 0.5 ml CDCl3 2,2',2''-nitrilotriethanol Assign. Shift(ppm)
A 4.6 B 3.617 C 2.603
Hz ppm Int.
410.56 4.585 122 329.38 3.678 759 327.38 3.656 337 324.69 3.626 984 323.44 3.612 744 321.38 3.589 400 319.63 3.569 1000 312.63 3.491 46 310.81 3.471 35 249.13 2.782 38 248.75 2.778 38 248.19 2.772 36 247.31 2.762 35 245.88 2.746 40 243.88 2.724 57 242.44 2.708 60 237.75 2.655 936 235.94 2.635 387 233.94 2.613 660 232.69 2.599 951 230.06 2.569 348 228.00 2.546 752
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