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1,3-Bis(2-hydroxyethoxy)benzene

Product Name 1,3-Bis(2-hydroxyethoxy)benzene

CAS102-40-9

MFC10H14O4

MW198.22

¹³CNMR

Mass

MS-IW-6470          
2,2'-(m-phenylenedioxy)diethanol
C10H14O4            (Mass of molecular ion:    198)

   Source Temperature: 150 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      15.0       1.2
      18.0       4.5
      19.0       1.4
      27.0       4.7
      28.0       1.1
      29.0       6.4
      31.0       1.2
      38.0       1.2
      39.0       5.3
      41.0       1.0
      42.0       1.4
      43.0       7.0
      44.0       6.3
      45.0      20.9
      50.0       1.9
      51.0       2.1
      52.0       1.0
      53.0       3.2
      54.0       1.4
      55.0       1.8
      63.0       3.7
      64.0       4.6
      65.0      15.1
      66.0       2.0
      67.0       1.4
      68.0       1.3
      69.0       5.7
      76.0       3.0
      77.0       3.0
      78.0       1.0
      79.0       2.0
      81.0       5.6
      82.0      17.5
      83.0       3.1
      91.0       1.2
      92.0       2.9
      93.0      10.0
      94.0       3.2
      95.0       3.1
     107.0       4.9
     108.0       1.5
     109.0       2.9
     110.0     100.0
     111.0      91.6
     112.0       6.3
     119.0       1.0
     121.0       1.0
     123.0       7.2
     124.0       3.6
     134.0       2.3
     135.0       4.6
     136.0       7.5
     137.0      14.9
     138.0       1.6
     153.0       1.5
     154.0      26.9
     155.0      34.5
     156.0       3.2
     180.0       2.4
     198.0      84.2
     199.0      10.0
     200.0       1.2

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₀ H₁₄ O₄	0.041 g : 0.5 ml DMSO-d₆
2,2'-(m-phenylenedioxy)diethanol

    Assign.     Shift(ppm)

      A             7.160
      B             6.51
      C             6.49
      D             4.86
      E             3.958
      F             3.709

     Hz     ppm     Int.

   2870.73   7.184    163
   2870.12   7.182    148
   2862.18   7.162    399
   2854.49   7.143    202
   2854.13   7.142    204
   2607.18   6.524    453
   2604.86   6.518    568
   2599.49   6.505    172
   2598.51   6.502    240
   2596.80   6.498    761
   2595.46   6.495    323
   2594.85   6.493    365
   2593.14   6.489    329
   2590.70   6.483    127
   1948.49   4.876    406
   1942.99   4.862    986
   1937.50   4.848    429
   1587.28   3.972    608
   1582.40   3.960   1000
   1579.96   3.954    240
   1577.15   3.947    734
   1489.62   3.728    366
   1484.25   3.714    787
   1479.49   3.702    648
   1474.00   3.689    297

in DMSO-d6

KBr disc

nujol mull

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