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N-Ethyl-3-methylaniline

Product Name N-Ethyl-3-methylaniline

CAS102-27-2

MFC9H13N

MW135.21

¹³CNMR

Mass

MS-NW-0560          
N-ethyl-m-toluidine
C9H13N              (Mass of molecular ion:    135)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.6
      28.0       1.8
      29.0       1.6
      39.0       5.0
      41.0       2.7
      42.0       1.6
      43.0       1.6
      50.0       1.5
      51.0       3.2
      52.0       1.8
      53.0       1.3
      58.5       1.0
      59.5       1.8
      60.0       1.5
      63.0       2.6
      64.0       1.0
      65.0       7.7
      77.0       6.6
      78.0       2.4
      79.0       2.9
      80.0       1.0
      89.0       2.0
      90.0       1.5
      91.0      17.8
      92.0       5.0
      93.0       3.3
     104.0       1.4
     105.0       1.1
     106.0       2.2
     117.0       1.0
     118.0       3.7
     119.0       3.2
     120.0     100.0
     121.0       9.3
     134.0       6.6
     135.0      37.2
     136.0       3.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₃ N	0.05 ml : 0.5 ml CDCl₃
N-ethyl-m-toluidine

    Assign.     Shift(ppm)

      A             7.038
      B             6.502
      C             6.387
      D             6.38
      E             3.33
      F             3.084
      G             2.254
      J             1.186

     Hz     ppm     Int.

   2821.29   7.060    104
   2818.97   7.054     48
   2813.84   7.041    144
   2812.50   7.038    124
   2811.16   7.035     57
   2807.62   7.026     33
   2805.05   7.019    132
   2602.66   6.513    138
   2602.17   6.512    135
   2594.97   6.494    127
   2594.24   6.492    114
   2552.86   6.388    330
   2546.26   6.372    125
   2543.95   6.366     67
   1332.40   3.334     36
   1243.41   3.112    173
   1236.33   3.094    484
   1229.13   3.076    482
   1221.92   3.058    176
    901.12   2.255   1000
    481.08   1.204    571
    474.00   1.187    960
    466.80   1.169    511

in CDCl3

CCl4 solution

liquid film

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N-Ethyl-3-methylaniline(102-27-2)¹HNMR Atlas of Related Products

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