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101-96-2More Spectrum > N,N'-Di-sec-butyl-p-phenylenediamine(101-96-2)MS
N,N'-Di-sec-butyl-p-phenylenediamine
Product Name N,N'-Di-sec-butyl-p-phenylenediamine
CAS101-96-2
MFC14H24N2
MW220.35
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MassMS-IW-5650 N,N'-di-sec-butyl-p-phenylenediamine C14H24N2 (Mass of molecular ion: 220)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.1 28.0 1.4 29.0 3.4 39.0 1.4 41.0 3.5 42.0 1.2 53.0 1.0 57.0 1.7 65.0 2.0 73.0 1.1 74.0 3.3 77.0 1.1 79.0 1.3 80.0 4.3 81.0 13.9 81.5 1.6 88.0 2.0 91.0 1.8 92.0 1.9 93.0 2.2 106.0 2.1 107.0 14.9 108.0 2.4 117.0 1.2 118.0 4.8 119.0 5.0 120.0 9.8 121.0 1.0 132.0 1.5 133.0 3.4 134.0 3.3 135.0 4.8 147.0 2.0 161.0 6.6 162.0 1.6 163.0 7.3 164.0 1.7 175.0 2.5 189.0 4.9 190.0 2.2 191.0 100.0 192.0 14.1 205.0 13.7 206.0 2.1 218.0 1.6 219.0 3.2 220.0 37.5 221.0 6.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H24 N2 0.05 ml : 0.5 ml CDCl3 N,N'-di-sec-butyl-p-phenylenediamine 
Assign. Shift(ppm)
A 6.514 B 3.259 C 2.96 D *1 1.580 E *1 1.404 F 1.123 G 0.928
Hz ppm Int.2603.76 6.516 962 1312.13 3.284 58 1305.91 3.268 101 1299.93 3.253 103 1293.70 3.238 62 1181.64 2.957 76 646.12 1.617 52 640.63 1.603 66 638.67 1.599 61 634.64 1.588 43 632.93 1.584 98 627.20 1.570 80 625.12 1.565 84 619.75 1.551 74 617.68 1.546 33 574.34 1.438 85 567.14 1.420 127 560.55 1.403 99 559.94 1.402 109 553.59 1.386 92 546.39 1.368 66 452.03 1.132 1000 445.80 1.116 976 442.02 1.107 43 382.20 0.957 36 378.30 0.947 505 370.85 0.928 932 363.40 0.910 435
in CDCl3
liquid film
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