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MassMS-IW-6667 3-methoxydiphenylamine C13H13NO (Mass of molecular ion: 199)
Source Temperature: 130 °C Sample Temperature: 110 °C Direct, 75 eV
39.0 1.2 51.0 2.9 52.0 1.1 63.0 1.8 64.0 1.9 65.0 1.7 66.0 1.0 77.0 4.8 78.0 1.1 83.5 1.9 92.0 5.5 93.0 1.0 99.5 3.2 115.0 1.0 127.0 2.0 128.0 4.0 129.0 4.8 130.0 1.2 154.0 6.4 155.0 3.9 156.0 4.5 157.0 1.1 166.0 3.1 167.0 7.5 168.0 7.8 169.0 3.7 170.0 7.5 171.0 1.0 183.0 6.3 184.0 3.1 198.0 9.5 199.0 100.0 200.0 14.7 201.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H13 N O 0.040 g : 0.5 ml CDCl3 3-methoxydiphenylamine 
Assign. Shift(ppm)
A 7.252 B 7.148 C 7.072 D 6.928 E 6.64 F 6.62 G 6.471 J 5.69 K 3.752
Hz ppm Int.2906.98 7.274 109 2906.25 7.272 50 2905.03 7.269 44 2900.51 7.258 63 2899.66 7.256 155 2898.44 7.253 173 2896.48 7.248 31 2893.19 7.240 53 2891.97 7.237 61 2891.11 7.235 154 2865.72 7.171 60 2858.76 7.154 46 2857.30 7.150 117 2856.57 7.148 89 2849.98 7.132 59 2849.12 7.130 70 2832.40 7.088 32 2831.54 7.086 42 2830.57 7.083 169 2829.35 7.080 200 2828.61 7.078 107 2827.27 7.075 56 2823.85 7.066 53 2822.88 7.064 87 2821.90 7.061 159 2820.80 7.059 140 2776.86 6.949 38 2775.76 6.946 67 2774.66 6.943 39 2769.41 6.930 53 2768.43 6.928 115 2767.58 6.926 52 2762.21 6.912 33 2761.11 6.909 56 2760.01 6.907 30 2656.62 6.648 52 2655.76 6.646 61 2654.42 6.642 85 2653.56 6.640 88 2649.05 6.629 83 2647.58 6.625 239 2646.73 6.623 145 2646.00 6.621 208 2644.53 6.618 62 2591.55 6.485 64 2590.70 6.483 68 2589.11 6.479 61 2588.26 6.477 60 2583.37 6.465 60 2581.79 6.461 83 2580.08 6.456 53 1499.88 3.753 1000
in CDCl3
KBr disc
nujol mull
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