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MassMS-NW-8385 3-phenylpyridine C11H9N (Mass of molecular ion: 155)
Source Temperature: 250 °C Sample Temperature: 140 °C Reservoir, 75 eV
18.0 1.2 39.0 2.7 50.0 4.7 51.0 9.3 52.0 2.6 62.0 1.7 63.0 4.9 64.0 5.0 74.0 3.2 75.0 3.5 76.0 5.1 77.0 5.6 77.5 1.8 78.0 2.3 87.0 1.1 89.0 1.1 101.0 2.2 102.0 10.0 103.0 1.4 115.0 2.9 126.0 3.7 127.0 11.3 128.0 9.6 129.0 2.9 140.0 1.3 153.0 2.2 154.0 38.9 155.0 100.0 156.0 12.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H9 N 0.05 ml : 0.5 ml CDCl3 3-phenylpyridine 
Assign. Shift(ppm)
A 8.836 B 8.565 C 7.817 D 7.537 E 7.439 F 7.372 G 7.306
Hz ppm Int.3532.47 8.839 321 3530.88 8.835 326 3425.05 8.571 232 3421.39 8.561 235 3420.41 8.559 228 3130.25 7.833 245 3128.54 7.829 296 3127.93 7.827 289 3126.22 7.823 243 3122.31 7.813 271 3120.61 7.809 317 3120.00 7.807 318 3118.29 7.803 258 3018.43 7.553 523 3016.97 7.550 781 3015.01 7.545 215 3011.35 7.535 410 3010.01 7.532 887 3009.52 7.531 757 3008.79 7.529 827 3006.71 7.524 128 2981.45 7.461 299 2980.35 7.458 505 2978.52 7.453 177 2973.14 7.440 1000 2971.68 7.436 484 2969.48 7.431 50 2967.04 7.425 276 2965.58 7.421 534 2963.50 7.416 92 2953.00 7.389 248 2951.66 7.386 458 2950.32 7.383 251 2946.66 7.374 165 2944.34 7.368 473 2941.89 7.362 115 2938.35 7.353 103 2937.01 7.349 171 2935.79 7.346 90 2926.51 7.323 268 2925.90 7.322 269 2921.75 7.311 272 2921.02 7.309 271 2918.70 7.304 261 2917.97 7.302 260 2913.82 7.291 251 2913.09 7.290 247
in CDCl3
liquid film
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