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3-Pyridinemethanol

Product Name 3-Pyridinemethanol

CAS100-55-0

MFC6H7NO

MW109.13

¹³CNMR

Mass

MS-NW-1119          
3-pyridinemethanol
C6H7NO              (Mass of molecular ion:    109)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      18.0       2.7
      26.0       4.7
      27.0      13.6
      28.0       5.6
      29.0       7.4
      31.0       8.2
      37.0       3.5
      38.0       7.1
      39.0      23.5
      40.0       2.2
      41.0       3.2
      49.0       2.4
      50.0      12.1
      51.0      23.9
      52.0      16.0
      53.0      34.4
      54.0       7.5
      55.0       4.9
      61.0       1.4
      62.0       2.6
      63.0       7.7
      64.0       9.9
      65.0      14.6
      66.0       1.7
      75.0       1.0
      76.0       1.1
      78.0      15.6
      79.0       9.4
      80.0      88.3
      81.0      14.7
      82.0       1.8
      91.0      20.1
      92.0       9.7
      93.0       2.0
     106.0       3.5
     107.0       2.9
     108.0      94.9
     109.0     100.0
     110.0       6.9

90 MHz in CDCl3

parameter in DMSO-d6

¹H NMR	89.56 MHz
C₆ H₇ N O	0.04 ml : 0.5 ml CDCl₃
3-pyridinemethanol

    Assign.     Shift(ppm)

      A             8.439
      B             8.360
      C             7.708
      D             7.259
      E             5.531
      F             4.67

     Hz     ppm     Int.

    757.19   8.455    248
    756.44   8.447    252
    755.63   8.438    231
    755.00   8.431    281
    754.25   8.422    250
    751.88   8.396    194
    750.19   8.377    198
    747.00   8.341    199
    745.31   8.322    205
    696.94   7.782     83
    695.19   7.763    125
    694.69   7.757    122
    693.00   7.738     83
    689.06   7.694    122
    687.44   7.676    180
    686.81   7.669    173
    686.19   7.662    107
    685.13   7.650    110
    655.75   7.322    236
    654.94   7.313    164
    650.88   7.268    163
    650.06   7.259    147
    648.00   7.236    126
    647.13   7.226    115
    643.06   7.181    116
    642.31   7.172    103
    495.38   5.532    351
    418.56   4.674   1000

¹H NMR	300 MHz
C₆ H₇ N O	30 % in DMSO
3-pyridinemethanol

    Parameter     ppm  Hz

      D(A)         8.70
      D(B)         7.90
      D(C)         7.42
      D(D)         8.55
       J(A,B)          2.0
       J(A,C)          1.0
       J(A,D)          0.0
       J(B,C)          7.1
       J(B,D)          1.4
       J(C,D)          4.4
     
      D(E)         4.69
     
      D(F)         5.58
     
     BRUEGEL,W. Z.ELEKTROCHEM.(BER.BUNSENGES.PHYS.CHEM.)
     66, 159 (1962)

     Hz     ppm     Int.

   2611.45   8.705    162
   2610.51   8.702    182
   2609.53   8.698    184
   2608.59   8.695    165
   2567.91   8.560    140
   2566.56   8.555    144
   2563.51   8.545    146
   2562.16   8.541    145
   2375.34   7.918     73
   2373.80   7.913     98
   2371.95   7.906     73
   2368.23   7.894     82
   2366.69   7.889    109
   2364.88   7.883     78
   2232.09   7.440     83
   2231.23   7.437     84
   2227.73   7.426     84
   2226.79   7.423     86
   2225.06   7.417     82
   2224.12   7.414     78
   2220.62   7.402     74
   2219.72   7.399     73
   1673.99   5.580    500
   1407.01   4.690   1000

in CDCl3

liquid film

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