CAS No. | 37148-48-4 |
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Molecular Formula | C8H7Cl2NO |
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Molecular Weight | 204.05300 |
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PSA | 43.09000 |
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LogP | 3.35940 |
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Appearance & Physical State | white to light yellow crystal powder |
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Density | 1.386g/cm3 |
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Boiling Point | 351.5ºC at 760mmHg |
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Melting Point | 161-165ºC |
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Flash Point | 166.4ºC |
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Refractive Index | 1.599 |
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Production method: amino acetophenone was obtained by chlorination. Add p-aminoacetophenone and acetic acid (80%) to the reaction pot, stir and dissolve, quickly add the chlorine-containing acetic acid solution, the feeding temperature is 5℃, add up, immediately put into the ice water precipitation, filter, wash, the obtained crude product with ethanol recrystalization, ready to get the finished product.
Chemical properties: beige crystal. Melting point 158-160℃. Insoluble in cold water, slightly soluble in hot water, easily soluble in ethanol, ether, benzene and other organic solvents.
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