1. Product information
| Product Name: | 2-Methoxybenzonitrile |
| Synonyms: | O-CYANOANISOLE;O-METHOXYBENZONITRILE;1-Cyano-2-methoxybenzene;2-Methoxybenzonitrile,98%;2-Cyanoanisole, o-Anisonitrile;AKOS B005792;AKOS 91422;2-METHOXYBENZONITRILE |
| CAS: | 6609-56-9 |
| MF: | C8H7NO |
| MW: | 133.15 |
| EINECS: | 229-559-0 |
| Product Categories: | Aromatic Nitriles;Nitriles;C8 to C9;Cyanides/Nitriles;Nitrogen Compounds |
| Mol File: | 6609-56-9.mol |
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| 2-Methoxybenzonitrile Chemical Properties |
| Melting point | 24.5°C |
| Boiling point | 135 °C12 mm Hg(lit.) |
| density | 1.093 g/mL at 25 °C(lit.) |
| refractive index | n20/D 1.5465(lit.) |
| Fp | >230 °F |
| storage temp. | Sealed in dry,Room Temperature |
| Water Solubility | Slightly soluble in water |
| form | Liquid |
| color | Clear colorless to pale yellow |
| 2-Methoxybenzonitrile Usage And Synthesis |
| Chemical Properties | Colorless liquid |
| Uses | 2-Methoxybenzonitrile was used in the synthesis of 5-(4′-methyl [1,1′-biphenyl]-2-yl)-1H-tetrazole. |
| Preparation | o-Anisidine with sodium nitrite to make a diazonium salt solution, add it to the lead cyanide solution, and then add benzene. Put the mixture for 10-15h and carry out steam distillation, separate the benzene layer from the distillate, dry it with calcium chloride, evaporate the benzene, and distill the residue under reduced pressure, collect 120-122.5°C (1.2kPa fraction) to get 2-Methoxybenzonitrile, yield 64.5-67.3%. |
| Synthesis Reference(s) | Journal of the American Chemical Society, 77, p. 109, 1955 DOI: 10.1021/ja01606a035
Synthesis, p. 641, 1992
Tetrahedron Letters, 32, p. 1007, 1991 DOI: 10.1016/S0040-4039(00)74473-X |
| General Description | Surface-enhanced Raman spectra study of 2-methoxybenzonitrile has been reported. |
2. Packaging
For powders: normal is 25kgs/Drum or bag, or larger/smaller package as request.
For liquids: normal 25kgs/drum, 180-300kgs/bucket, or IBC, determined by the nature of the product.
Or smaller package 1kg/bottle, 10kgs/bottle as request.
3. Shipping
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