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3,3,5,5-TETRAMETHYLCYCLOHEXANONE

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3,3,5,5-TETRAMETHYLCYCLOHEXANONE Basic information
3,3,5,5-TETRAMETHYLCYCLOHEXANONE Chemical Properties
  • Melting point:11-12 °C
  • Boiling point:200-203 °C
  • Density 0.881 g/mL at 25 °C (lit.)
  • refractive index n20/D 1.451(lit.)
  • Flash point:164 °F
  • storage temp. Sealed in dry,Room Temperature
  • form Liquid
  • color Clear colorless to slightly yellow
  • BRN 1237421
  • InChIKeyOQJMHUOCLRCSED-UHFFFAOYSA-N
  • CAS DataBase Reference14376-79-5(CAS DataBase Reference)
Safety Information
  • Safety Statements 23-24/25
  • WGK Germany 3
  • HS Code 29142990
MSDS
3,3,5,5-TETRAMETHYLCYCLOHEXANONE Usage And Synthesis
  • Chemical PropertiesClear colorless to slightly yellow liquid
  • Synthesis Reference(s)Tetrahedron Letters, 25, p. 3463, 1984 DOI: 10.1016/S0040-4039(01)91048-2
  • Purification MethodsPurify the ketone first through a 24inch column packed with Raschig rings, then a 40cm Vigreux column (p 11) under reduced pressure (b 69-69.3o/7mm, see above). The oxime has m 144-145o (from 60% EtOH), and the semicarbazone has m 196-197o, 197-198o (214.5o, 217-218o) [Karasch & Tawney J Am Chem Soc 63 2308 1941, UV: Sandris & Ourisson Bull Soc Chim Fr 958 1956]. [Beilstein 7 III 163, 7 IV 89.]
3,3,5,5-TETRAMETHYLCYCLOHEXANONE(14376-79-5)Related Product Information
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