2-(3-브로모페닐)-4,6-디페닐-1,3,5-트리아진

그림문자(GHS)

• 그림문자(GHS)

  

• 신호 어

  Warning

• 유해·위험 문구

  H315：피부에 자극을 일으킴

  H319：눈에 심한 자극을 일으킴

• 예방조치문구

  P264：취급 후에는 손을 철저히 씻으시오.

  P264：취급 후에는 손을 철저히 씻으시오.

  P280：보호장갑/보호의/보안경/안면보호구를 착용하시오.

  P302+P352：피부에 묻으면 다량의 물로 씻으시오.

  P305+P351+P338：눈에 묻으면 몇 분간 물로 조심해서 씻으시오. 가능하면 콘택트렌즈를 제거하시오. 계속 씻으시오.

  P321：(…) 처치를 하시오.

  P332+P313：피부 자극이 생기면 의학적인 조치· 조언을 구하시오.

  P362：오염된 의복을 벗고 세척 후에 재사용하기

2-(3-브로모페닐)-4,6-디페닐-1,3,5-트리아진 화학적 특성, 용도, 생산

• 화학적 성질

  white powder

• 주요 응용

  2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine (BPTPT) is a white powder that is insoluble in water. It has a variety of applications in organic synthesis, most commonly as an intermediate in the synthesis of other compounds.

• Synthesis

  A compound, 2-chloro-4,6-diphenyl-1,3,5-triazine (50 g, 187 mmol, TCI) was dissolved in THF (1 L) under a nitrogen environment, (3-bromophenyl)boronic acid (45 g, 224.12 mmol) and tetrakis(triphenylphosphine)palladium (2.1 g, 1.87 mmol) were added thereto, and the mixture was stirred. Potassium carbonate saturated in water (64 g, 467 mmol) was added thereto, and the obtained mixture was heated and refluxed at 80° C. for 12 hours. When the reaction was complete, water was added to the reaction solution, and the mixture was extracted with dichloromethane (DCM) and then filtered after removing moisture with anhydrous MgSO4 and concentrated under a reduced pressure. The obtained residue was separated and purified through column chromatography to obtain 2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine (69 g, 95 percent).

2-(3-브로모페닐)-4,6-디페닐-1,3,5-트리아진 준비 용품 및 원자재

2-(3-브로모페닐)-4,6-디페닐-1,3,5-트리아진 공급 업체

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